3,6-di-tert-butyl-2,2,7-trifluoro-1-(2,6-diisopropylephenyl)-1,3,5-triaza-7-bora-2-sila-1,2,3,4-cyclohepten

Base Information

Chemical Name:3,6-di-tert-butyl-2,2,7-trifluoro-1-(2,6-diisopropylephenyl)-1,3,5-triaza-7-bora-2-sila-1,2,3,4-cyclohepten
CAS No.:1239598-00-5
Molecular Formula:C₂₂H₃₇BF₃N₃Si
Molecular Weight:439.448
Hs Code.:

Synonyms:3,6-di-tert-butyl-2,2,7-trifluoro-1-(2,6-diisopropylephenyl)-1,3,5-triaza-7-bora-2-sila-1,2,3,4-cyclohepten

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Chemical Property of 3,6-di-tert-butyl-2,2,7-trifluoro-1-(2,6-diisopropylephenyl)-1,3,5-triaza-7-bora-2-sila-1,2,3,4-cyclohepten

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Technology Process of 3,6-di-tert-butyl-2,2,7-trifluoro-1-(2,6-diisopropylephenyl)-1,3,5-triaza-7-bora-2-sila-1,2,3,4-cyclohepten

There total 2 articles about 3,6-di-tert-butyl-2,2,7-trifluoro-1-(2,6-diisopropylephenyl)-1,3,5-triaza-7-bora-2-sila-1,2,3,4-cyclohepten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: (2-diisopropylanilino-2-fluoro-1,3-diaza-2-silacyclopentene)lithium(THF)2

: 1239598-00-5
3,6-di-tert-butyl-2,2,7-trifluoro-1-(2,6-diisopropylephenyl)-1,3,5-triaza-7-bora-2-sila-1,2,3,4-cyclohepten

Guidance literature:: With boron trifluoride diethyl etherate; In tetrahydrofuran; hexane; at 0 ℃; Reflux; Inert atmosphere;
DOI:10.1002/zaac.200900341

Reference yield: 95.0%

: (2-diisopropylanilino-2-fluoro-1,3-diaza-2-silacyclopentene)lithium(THF)2

: 109-63-7
boron trifluoride diethyl etherate

: 1239598-00-5
3,6-di-tert-butyl-2,2,7-trifluoro-1-(2,6-diisopropylephenyl)-1,3,5-triaza-7-bora-2-sila-1,2,3,4-cyclohepten

Guidance literature:: In tetrahydrofuran; hexane; byproducts: LiF, THF, OEt2; under N2, to soln. of (HCNCMe3)2Si(F)N(C6H3(CH(CH3)2))Li(THF)2 added equimolar amount of BF3*Et2O at 0°C, refluxed for 3 h; solvent removed (in vac.), recrystd. from hexane;
DOI:10.1002/zaac.200900341