3,5-dicyano-4-phenyl-2,6-pyridione

Base Information

• Chemical Name: 3,5-dicyano-4-phenyl-2,6-pyridione
• CAS No.: 854389-36-9
• Molecular Formula: C₁₃H₇N₃O₂
• Molecular Weight: 237.217
• Mol file: 854389-36-9.mol

Synonyms:3,5-dicyano-4-phenyl-2,6-pyridione

Chemical Property of 3,5-dicyano-4-phenyl-2,6-pyridione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,5-dicyano-4-phenyl-2,6-pyridione

There total 4 articles about 3,5-dicyano-4-phenyl-2,6-pyridione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-phenyl-3,5-dicyano-2,6-piperidinedione → 3,5-dicyano-4-phenyl-2,6-pyridione (854389-36-9)

Guidance literature:

With oxygen; copper(II) acetate monohydrate; In ethanol; for 2h; Reflux;

Reference yield:

C13H12N4O2 → 3,5-dicyano-4-phenyl-2,6-pyridione (854389-36-9)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 1.5 h

2: copper(II) acetate monohydrate; oxygen / ethanol / 2 h / Reflux

With oxygen; copper(II) acetate monohydrate; In ethanol;

Reference yield:

benzaldehyde (100-52-7) → 3,5-dicyano-4-phenyl-2,6-pyridione (854389-36-9)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium hydroxide / ethanol / 2.5 h / 90 °C

2: sodium hydroxide / ethanol / 1 h

3: ethanol / 1.5 h

4: copper(II) acetate monohydrate; oxygen / ethanol / 2 h / Reflux

With oxygen; copper(II) acetate monohydrate; sodium hydroxide; In ethanol;

upstream raw materials:

benzaldehyde

2-cyano-3-phenylacrylamide

Downstream raw materials:

3,5-dicyano-4-phenyl-2,6-didicambyl pyridione