6-(4-(4-methyl-1H-5-carboxylic acid 1,2,3-triazol-1-yl)phenylamino)phenyl-N⁽²⁾,N⁽⁴⁾-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine

Base Information

• Chemical Name: 6-(4-(4-methyl-1H-5-carboxylic acid 1,2,3-triazol-1-yl)phenylamino)phenyl-N⁽²⁾,N⁽⁴⁾-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine
• CAS No.: 1417999-99-5
• Molecular Formula: C₂₇H₂₅N₉O₄
• Molecular Weight: 539.553

Synonyms:6-(4-(4-methyl-1H-5-carboxylic acid 1,2,3-triazol-1-yl)phenylamino)phenyl-N⁽²⁾,N⁽⁴⁾-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine

Chemical Property of 6-(4-(4-methyl-1H-5-carboxylic acid 1,2,3-triazol-1-yl)phenylamino)phenyl-N⁽²⁾,N⁽⁴⁾-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine

Chemical Property:

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Technology Process of 6-(4-(4-methyl-1H-5-carboxylic acid 1,2,3-triazol-1-yl)phenylamino)phenyl-N⁽²⁾,N⁽⁴⁾-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine

There total 4 articles about 6-(4-(4-methyl-1H-5-carboxylic acid 1,2,3-triazol-1-yl)phenylamino)phenyl-N⁽²⁾,N⁽⁴⁾-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

C23H21N9O2 (1417999-98-4) + ethyl acetoacetate (141-97-9) → 6-(4-(4-methyl-1H-5-carboxylic acid 1,2,3-triazol-1-yl)phenylamino)phenyl-N(2),N(4)-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine (1417999-99-5)

Guidance literature:

With sodium acetate; In ethanol; at 20 ℃; for 1h;

Reference yield:

4-methoxy-aniline (104-94-9) → 6-(4-(4-methyl-1H-5-carboxylic acid 1,2,3-triazol-1-yl)phenylamino)phenyl-N(2),N(4)-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine (1417999-99-5)

Guidance literature:

Multi-step reaction with 4 steps

1.1: 3 h / 20 °C

2.1: sodium carbonate / 4 h / 35 - 50 °C

3.1: hydrogenchloride; sodium nitrite / water / 0.17 h / 0 °C

3.2: 3 h / 0 °C

4.1: sodium acetate / ethanol / 1 h / 20 °C

With hydrogenchloride; sodium acetate; sodium carbonate; sodium nitrite; In ethanol; water;

Reference yield:

4,6-dichloro-N-(4-methoxyphenyl)-1,3,5-triazin-2-amine (30377-27-6) → 6-(4-(4-methyl-1H-5-carboxylic acid 1,2,3-triazol-1-yl)phenylamino)phenyl-N(2),N(4)-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine (1417999-99-5)

Guidance literature:

Multi-step reaction with 4 steps

1.1: 3 h / 20 °C

2.1: sodium carbonate / 4 h / 35 - 50 °C

3.1: hydrogenchloride; sodium nitrite / water / 0.17 h / 0 °C

3.2: 3 h / 0 °C

4.1: sodium acetate / ethanol / 1 h / 20 °C

With hydrogenchloride; sodium acetate; sodium carbonate; sodium nitrite; In ethanol; water;

upstream raw materials:

C₂₃H₂₁N₉O₂

ethyl acetoacetate

4,6-dichloro-N-(4-methoxyphenyl)-1,3,5-triazin-2-amine

4-methoxy-aniline

Downstream raw materials:

6-(4-(4-methyl-1H-5-carbonylchloride-1,2,3-triazol-1ylphenylamino)phenyl)-N⁽²⁾,N⁽⁴⁾-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine

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