(4-(2-chloro-4-nitrophenyl)piperazin-1-yl)(4-(2-methoxyphenyl)-1-methyl-1H-1,2,3-triazol-5-yl)methanone

Base Information

Chemical Name:(4-(2-chloro-4-nitrophenyl)piperazin-1-yl)(4-(2-methoxyphenyl)-1-methyl-1H-1,2,3-triazol-5-yl)methanone
CAS No.:1370420-13-5
Molecular Formula:C₂₁H₂₁ClN₆O₄
Molecular Weight:456.889
Hs Code.:

Synonyms:(4-(2-chloro-4-nitrophenyl)piperazin-1-yl)(4-(2-methoxyphenyl)-1-methyl-1H-1,2,3-triazol-5-yl)methanone

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Chemical Property of (4-(2-chloro-4-nitrophenyl)piperazin-1-yl)(4-(2-methoxyphenyl)-1-methyl-1H-1,2,3-triazol-5-yl)methanone

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Technology Process of (4-(2-chloro-4-nitrophenyl)piperazin-1-yl)(4-(2-methoxyphenyl)-1-methyl-1H-1,2,3-triazol-5-yl)methanone

There total 4 articles about (4-(2-chloro-4-nitrophenyl)piperazin-1-yl)(4-(2-methoxyphenyl)-1-methyl-1H-1,2,3-triazol-5-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: C₁₁H₁₀ClN₃O₂

: 114878-60-3
1-(2-chloro-4-nitro-phenyl)piperazine

: 1370420-13-5
(4-(2-chloro-4-nitrophenyl)piperazin-1-yl)(4-(2-methoxyphenyl)-1-methyl-1H-1,2,3-triazol-5-yl)methanone

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;

Reference yield:

: C₁₀H₁₁N₃O

: 1370420-13-5
(4-(2-chloro-4-nitrophenyl)piperazin-1-yl)(4-(2-methoxyphenyl)-1-methyl-1H-1,2,3-triazol-5-yl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1.33 h / -75 °C / Inert atmosphere

1.2: -75 - 20 °C

2.1: thionyl chloride / 5 h / Reflux

3.1: triethylamine / dichloromethane / 20 °C

With thionyl chloride; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1364523-68-1
1-methyl-4-(2-methoxyphenyl)-[1,2,3]triazole-5-carboxylic acid

: 1370420-13-5
(4-(2-chloro-4-nitrophenyl)piperazin-1-yl)(4-(2-methoxyphenyl)-1-methyl-1H-1,2,3-triazol-5-yl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 5 h / Reflux

2: triethylamine / dichloromethane / 20 °C

With thionyl chloride; triethylamine; In dichloromethane;