(S)-3-methyl-1,5-pentanediol monotosylate monobenzyl ether

Base Information

Chemical Name:(S)-3-methyl-1,5-pentanediol monotosylate monobenzyl ether
CAS No.:87106-24-9
Molecular Formula:C₂₀H₂₆O₄S
Molecular Weight:362.49
Hs Code.:

Synonyms:(S)-3-methyl-1,5-pentanediol monotosylate monobenzyl ether

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Chemical Property of (S)-3-methyl-1,5-pentanediol monotosylate monobenzyl ether

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Technology Process of (S)-3-methyl-1,5-pentanediol monotosylate monobenzyl ether

There total 3 articles about (S)-3-methyl-1,5-pentanediol monotosylate monobenzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87106-22-7
(R,E)-(+)-7-hydroxy-3,7-dimethyl-5-octenyl benzyl ether

: 87106-24-9
(S)-3-methyl-1,5-pentanediol monotosylate monobenzyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) ozone 2.) NaBH₄ / 1.) CH₂Cl₂, MeOH, -70 deg C, 2.) room temperature, overnight

2: 5.72 g / pyridine / 5 h / 0 - 5 °C

With sodium tetrahydroborate; ozone; In pyridine;
DOI:10.1016/S0040-4020(01)91971-4

Reference yield:

: 83541-12-2
(R)-(+)-citronellyl benzyl ether

: 87106-24-9
(S)-3-methyl-1,5-pentanediol monotosylate monobenzyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Ph₂Se₂, MgSO₄ 2.) 70percent t-BuOOH / 1.) CH₂Cl₂, 20 h, room temperature, 2.) room temperature, overnight

2: 1.) ozone 2.) NaBH₄ / 1.) CH₂Cl₂, MeOH, -70 deg C, 2.) room temperature, overnight

3: 5.72 g / pyridine / 5 h / 0 - 5 °C

With tert.-butylhydroperoxide; sodium tetrahydroborate; diphenyl diselenide; magnesium sulfate; ozone; In pyridine;
DOI:10.1016/S0040-4020(01)91971-4