Mo(CNC₆H₅)7⁽²⁺⁾*2PF₆^(1-)

Base Information

Chemical Name:Mo(CNC₆H₅)7⁽²⁺⁾*2PF₆^(1-)
CAS No.:78653-88-0
Molecular Formula:C₄₉H₃₅MoN₇*2F₆P
Molecular Weight:1107.73
Hs Code.:

Mo(CNC<sub>6</sub>H<sub>5</sub>)7<sup>(2+)</sup>*2PF<sub>6</sub><sup>(1-)</sup>

Synonyms:Mo(CNC₆H₅)7⁽²⁺⁾*2PF₆^(1-)

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Chemical Property of Mo(CNC₆H₅)7⁽²⁺⁾*2PF₆^(1-)

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Technology Process of Mo(CNC₆H₅)7⁽²⁺⁾*2PF₆^(1-)

There total 3 articles about Mo(CNC₆H₅)7⁽²⁺⁾*2PF₆^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 16921-91-8
nitrosyl hexafluorophosphate

: 14154-60-0
hexakis(phenylisocyanide)molybdenum⁽⁰⁾

: 78653-88-0
Mo(CNC₆H₅)7⁽²⁺⁾*2PF₆^(1-)

: 78653-92-6
[Mo(NO)(CNPh)5]PF₆

Guidance literature:: In tetrahydrofuran; hexane; under N2, first Mo(CNPh)6 was dissolved in THF, then NOPF6 was added tothe stirred soln., then addn. of hexane; filtration, solid prod. washed with diethyl ether, dried in vac., elem.anal.; filtrate was taken to dryness, recrystn. from acetone-diethyl ether, elem. anal.;

Reference yield: 81.0%

: 17084-13-8
potassium hexafluorophosphate

: 79721-70-3
[Mo(phenyl isocyanide)6Cl] hexafluorophosphate

: 1197040-29-1,931-54-4
phenyl isocyanate

: 78653-88-0
Mo(CNC₆H₅)7⁽²⁺⁾*2PF₆^(1-)

Guidance literature:: In ethanol; under N2, stirred at room temp. for 6 h; mixt. filtered, washed with water, 2-propanol, diethyl ether, dried in vac.;

Reference yield: 71.0%

: 17084-13-8
potassium hexafluorophosphate

: 14154-60-0
hexakis(phenylisocyanide)molybdenum⁽⁰⁾

: 1197040-29-1,931-54-4
phenyl isocyanate

: 78653-88-0
Mo(CNC₆H₅)7⁽²⁺⁾*2PF₆^(1-)

: 78653-92-6
[Mo(NO)(CNPh)5]PF₆

Guidance literature:: With silver nitrate; In acetone; under N2, stirred at room temp. for 3 h in the dark; mixt. filtered, pptd. with diethyl ether, prod. filtered, washed with water, 2-propanol, diethyl ether, recrystd. by dissolving the prod. in acetone then addn. of diethyl ether, elem.anal.;