5-[acetyl(toluene-4-sulfonyl)amino]4-ethoxythiocarbonylsulfanylpentanoic acid methyl ester

Base Information

Chemical Name:5-[acetyl(toluene-4-sulfonyl)amino]4-ethoxythiocarbonylsulfanylpentanoic acid methyl ester
CAS No.:851461-04-6
Molecular Formula:C₁₈H₂₅NO₆S₃
Molecular Weight:447.598
Hs Code.:

Synonyms:5-[acetyl(toluene-4-sulfonyl)amino]4-ethoxythiocarbonylsulfanylpentanoic acid methyl ester

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Chemical Property of 5-[acetyl(toluene-4-sulfonyl)amino]4-ethoxythiocarbonylsulfanylpentanoic acid methyl ester

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Technology Process of 5-[acetyl(toluene-4-sulfonyl)amino]4-ethoxythiocarbonylsulfanylpentanoic acid methyl ester

There total 4 articles about 5-[acetyl(toluene-4-sulfonyl)amino]4-ethoxythiocarbonylsulfanylpentanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 851460-96-3
4-ethoxythiocarbonylsulfanyl-5-(toluene-4-sulfonylamino)pentanoic acid methyl ester

: 108-24-7
acetic anhydride

: 851461-04-6
5-[acetyl(toluene-4-sulfonyl)amino]4-ethoxythiocarbonylsulfanylpentanoic acid methyl ester

Guidance literature:: With pyridine;
DOI:10.1016/j.tet.2007.04.091

Reference yield: 28.0%

: 123972-89-4
ethoxyrhiocarbonylsulfanylacetic acid methyl ester

: 154139-38-5
N-acetyl-N-allyl-4-methyl-benzenesulfonamide

: 851461-04-6
5-[acetyl(toluene-4-sulfonyl)amino]4-ethoxythiocarbonylsulfanylpentanoic acid methyl ester

Guidance literature:: With dilauryl peroxide; In 1,2-dichloro-ethane; Heating;
DOI:10.1016/j.tet.2007.04.091

Reference yield:

: 50487-71-3
4-methyl-N-(2-propenyl)benzenesulfonamide

: 851461-04-6
5-[acetyl(toluene-4-sulfonyl)amino]4-ethoxythiocarbonylsulfanylpentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / toluene / 48 h / Heating

2: 28 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

With dilauryl peroxide; In 1,2-dichloro-ethane; toluene;
DOI:10.1016/j.tet.2007.04.091