3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-1-O-(methylsulfonyl)propanol

Base Information

Chemical Name:3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-1-O-(methylsulfonyl)propanol
CAS No.:140909-66-6
Molecular Formula:C₃₈H₄₄O₈S
Molecular Weight:660.829
Hs Code.:

Synonyms:3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-1-O-(methylsulfonyl)propanol

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Chemical Property of 3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-1-O-(methylsulfonyl)propanol

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Technology Process of 3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-1-O-(methylsulfonyl)propanol

There total 4 articles about 3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-1-O-(methylsulfonyl)propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-63-0
methanesulfonyl chloride

: 141042-24-2
3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-1-propanol

: 140909-66-6
3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-1-O-(methylsulfonyl)propanol

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/0008-6215(92)80021-R

Reference yield:

: 82659-59-4
3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)propene

: 140909-66-6
3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-1-O-(methylsulfonyl)propanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 9-BBN, 2) 4M NaOH, 30percent H₂O₂ / 1) THF, refflux, 3 h, 2) EtOH, r.t., overnight

2: Et₃N / CH₂Cl₂ / 1 h / 0 °C

With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; triethylamine; In dichloromethane;
DOI:10.1016/0008-6215(92)80021-R

Reference yield:

: 82598-88-7
2,3,4,6-tetra-O-benzyl-D-mannono-1,5-lactone

: 140909-66-6
3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-1-O-(methylsulfonyl)propanol

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / -78 °C

2: Et₃SiH, BF₃OEt₂ / acetonitrile

3: 1) 9-BBN, 2) 4M NaOH, 30percent H₂O₂ / 1) THF, refflux, 3 h, 2) EtOH, r.t., overnight

4: Et₃N / CH₂Cl₂ / 1 h / 0 °C

With triethylsilane; sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; boron trifluoride diethyl etherate; dihydrogen peroxide; triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/0008-6215(92)80021-R