Technology Process of C33H61O8PSi2
There total 18 articles about C33H61O8PSi2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
dimethyl methane phosphonate;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 0.5h;
C31H56O6Si2;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 1h;
Further stages.;
DOI:10.1039/b602021f
- Guidance literature:
-
dimethyl methane phosphonate;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 0.5h;
C31H56O6Si2;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 1h;
Further stages. Title compound not separated from byproducts.;
DOI:10.1039/b602021f
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 25.84 g / imidazole; 4-DMAP / CH2Cl2 / 1.5 h / 25 °C
2.1: 78 percent / NaH2PO4; NaClO2; 2-methyl-2-butene / 2-methyl-propan-2-ol; H2O / 2 h / 25 °C
3.1: 97 percent / K2CO3 / acetone / 16 h / 25 °C
4.1: KHMDS / tetrahydrofuran; toluene / 0.5 h / -78 °C
4.2: Davis oxaziridine / tetrahydrofuran; toluene / 1 h / -78 °C
5.1: 86 percent / imidazole; 4-DMAP / CH2Cl2 / 16 h / 25 °C
6.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C
6.2: 92 percent / tetrahydrofuran; hexane / 1 h / -78 °C
With
1H-imidazole; dmap; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; potassium hexamethylsilazane; potassium carbonate;
In
tetrahydrofuran; hexane; dichloromethane; water; acetone; toluene; tert-butyl alcohol;
DOI:10.1039/b602021f
