5-(4-chloro-phenoxymethyl)-3-hydroxymethyl-3H-[1,3,4]oxadiazole-2-thione

Base Information

• Chemical Name: 5-(4-chloro-phenoxymethyl)-3-hydroxymethyl-3H-[1,3,4]oxadiazole-2-thione
• CAS No.: 68301-04-2
• Molecular Formula: C₁₀H₉ClN₂O₃S
• Molecular Weight: 272.712

Synonyms:5-(4-chloro-phenoxymethyl)-3-hydroxymethyl-3H-[1,3,4]oxadiazole-2-thione

Chemical Property of 5-(4-chloro-phenoxymethyl)-3-hydroxymethyl-3H-[1,3,4]oxadiazole-2-thione

Chemical Property:

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Technology Process of 5-(4-chloro-phenoxymethyl)-3-hydroxymethyl-3H-[1,3,4]oxadiazole-2-thione

There total 1 articles about 5-(4-chloro-phenoxymethyl)-3-hydroxymethyl-3H-[1,3,4]oxadiazole-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2-mercapto-5-((4-chlorophenoxy)methyl)-1,3,4-oxadiazole (62382-85-8) → 5-(4-chloro-phenoxymethyl)-3-hydroxymethyl-3H-[1,3,4]oxadiazole-2-thione (68301-04-2)

Guidance literature:

In ethanol; Ambient temperature;

Reference yield: 100.0%

tributyltin chloride (1461-22-9) + 5-(4-chloro-phenoxymethyl)-3-hydroxymethyl-3H-[1,3,4]oxadiazole-2-thione (68301-04-2) → (C4H9)3SnOCH2C2N2OSCH2OC6H4Cl (75543-24-7)

Guidance literature:

With K₂CO₃; In acetone; 1:1:1.5 mole ratio of Bu3SnCl, alc., and K2CO3; refluxing for 9 h;

Reference yield:

diethyl phosphorochloridothioate (2524-04-1) + 5-(4-chloro-phenoxymethyl)-3-hydroxymethyl-3H-[1,3,4]oxadiazole-2-thione (68301-04-2) → thiophosphoric acid O-[5-(4-chloro-phenoxymethyl)-2-thioxo-[1,3,4]oxadiazol-3-ylmethyl] ester O',O''-diethyl ester (68300-94-7)

Guidance literature:

With potassium carbonate; In acetone; Heating;

upstream raw materials:

formaldehyd

2-mercapto-5-((4-chlorophenoxy)methyl)-1,3,4-oxadiazole

Downstream raw materials:

thiophosphoric acid O-[5-(4-chloro-phenoxymethyl)-2-thioxo-[1,3,4]oxadiazol-3-ylmethyl] ester O',O''-diethyl ester

thiophosphoric acid O-[5-(4-chloro-phenoxymethyl)-2-thioxo-[1,3,4]oxadiazol-3-ylmethyl] ester O',O''-dipropyl ester

butylcarbamic acid 5-(4-chloro-phenoxymethyl)-2-thioxo-[1,3,4]oxadiazol-3-ylmethyl ester

thiophosphoric acid O,O'-dibutyl ester O''-[5-(4-chloro-phenoxymethyl)-2-thioxo-[1,3,4]oxadiazol-3-ylmethyl] ester

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