((CH₃)3C₆H₂)2GeNC(C₆H₅)C₁₃H₈

Base Information

• Chemical Name: ((CH₃)3C₆H₂)2GeNC(C₆H₅)C₁₃H₈
• CAS No.: 785805-40-5
• Molecular Formula: C₃₈H₃₅GeN
• Molecular Weight: 578.293
• Mol file: 785805-40-5.mol

Synonyms:((CH₃)3C₆H₂)2GeNC(C₆H₅)C₁₃H₈

Chemical Property of ((CH₃)3C₆H₂)2GeNC(C₆H₅)C₁₃H₈

Chemical Property:

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Technology Process of ((CH₃)3C₆H₂)2GeNC(C₆H₅)C₁₃H₈

There total 1 articles about ((CH₃)3C₆H₂)2GeNC(C₆H₅)C₁₃H₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

((CH3)3C6H2)2GeFCH(C13H9)2 + benzonitrile (100-47-0) → ((CH3)3C6H2)2GeNC(C6H5)C13H8 (785805-40-5)

Guidance literature:

With tert-butyllithium; In diethyl ether; pentane; byproducts: LiF; High Pressure; to germene (prepared by addn. t-BuLi in pentane to soln. fluorogermane in Et2O at -78°C followed by warming to room temp.) PhCN was addedat -78°C and stirred overnight at room temp.; ppt. was filtered, solvents were removed in vacuo, residue was crystd. from pentane at -20°C; elem. anal.;

DOI:10.1021/om0494622

upstream raw materials:

benzonitrile