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Technology Process of ((CH3)3C6H2)2GeNC(C6H5)C13H8

((CH3)3C6H2)2GeNC(C6H5)C13H8

Base Information
  • Chemical Name:((CH3)3C6H2)2GeNC(C6H5)C13H8
  • CAS No.:785805-40-5
  • Molecular Formula:C38H35GeN
  • Molecular Weight:578.293
  • Hs Code.:
((CH<sub>3</sub>)3C<sub>6</sub>H<sub>2</sub>)2GeNC(C<sub>6</sub>H<sub>5</sub>)C<sub>13</sub>H<sub>8</sub>

Synonyms:((CH3)3C6H2)2GeNC(C6H5)C13H8

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Chemical Property of ((CH3)3C6H2)2GeNC(C6H5)C13H8
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Technology Process of ((CH3)3C6H2)2GeNC(C6H5)C13H8

There total 1 articles about ((CH3)3C6H2)2GeNC(C6H5)C13H8 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

((CH<sub>3</sub>)3C<sub>6</sub>H<sub>2</sub>)2GeFCH(C<sub>13</sub>H<sub>9</sub>)2

((CH3)3C6H2)2GeFCH(C13H9)2

benzonitrile
100-47-0

benzonitrile

((CH<sub>3</sub>)3C<sub>6</sub>H<sub>2</sub>)2GeNC(C<sub>6</sub>H<sub>5</sub>)C<sub>13</sub>H<sub>8</sub>
785805-40-5

((CH3)3C6H2)2GeNC(C6H5)C13H8

Guidance literature:
With tert-butyllithium; In diethyl ether; pentane; byproducts: LiF; High Pressure; to germene (prepared by addn. t-BuLi in pentane to soln. fluorogermane in Et2O at -78°C followed by warming to room temp.) PhCN was addedat -78°C and stirred overnight at room temp.; ppt. was filtered, solvents were removed in vacuo, residue was crystd. from pentane at -20°C; elem. anal.;
DOI:10.1021/om0494622
upstream raw materials:

benzonitrile

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