4-chloro-2-[3-(tert-butyldimethylsilyloxymethyl)phenyl]-6-morpholinopyrimidine

Base Information

• Chemical Name: 4-chloro-2-[3-(tert-butyldimethylsilyloxymethyl)phenyl]-6-morpholinopyrimidine
• CAS No.: 941316-93-4
• Molecular Formula: C₂₁H₃₀ClN₃O₂Si
• Molecular Weight: 420.027

Synonyms:4-chloro-2-[3-(tert-butyldimethylsilyloxymethyl)phenyl]-6-morpholinopyrimidine

Chemical Property of 4-chloro-2-[3-(tert-butyldimethylsilyloxymethyl)phenyl]-6-morpholinopyrimidine

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Technology Process of 4-chloro-2-[3-(tert-butyldimethylsilyloxymethyl)phenyl]-6-morpholinopyrimidine

There total 1 articles about 4-chloro-2-[3-(tert-butyldimethylsilyloxymethyl)phenyl]-6-morpholinopyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-2-(3-hydroxymethylphenyl)-6-morpholinopyrimidine (873566-62-2) + tert-butyldimethylsilyl chloride (18162-48-6) → 4-chloro-2-[3-(tert-butyldimethylsilyloxymethyl)phenyl]-6-morpholinopyrimidine (941316-93-4)

Guidance literature:

With 1H-imidazole; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

4-chloro-2-[3-(tert-butyldimethylsilyloxymethyl)phenyl]-6-morpholinopyrimidine (941316-93-4) + tert-Butyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,6-dihydro-1(2H)-pyridinecarboxylate (375853-82-0,286961-14-6) → 4-(N-tert-butoxycarbonyl-1,2,3,6-tetrahydropyridin-4-yl)-2-[3-(tert-butyldimethylsilyloxymethyl)phenyl]-6-morpholinopyrimidine (941316-94-5)

Guidance literature:

With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water; at 80 ℃; for 4h;

upstream raw materials:

4-chloro-2-(3-hydroxymethylphenyl)-6-morpholinopyrimidine

tert-butyldimethylsilyl chloride

Downstream raw materials:

4-(N-tert-butoxycarbonyl-1,2,3,6-tetrahydropyridin-4-yl)-2-[3-(tert-butyldimethylsilyloxymethyl)phenyl]-6-morpholinopyrimidine

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