3-methyl-4,5,6,7-tetrahydro-1H-indazol-4-ol

Base Information

Chemical Name:3-methyl-4,5,6,7-tetrahydro-1H-indazol-4-ol
CAS No.:96546-41-7
Molecular Formula:C₈H₁₂N₂O
Molecular Weight:152.196
Hs Code.:2933990090
DSSTox Substance ID:DTXSID701262634
Mol file:96546-41-7.mol

Synonyms:3-methyl-4,5,6,7-tetrahydro-1H-indazol-4-ol;96546-41-7;DTXSID701262634;4,5,6,7-Tetrahydro-3-methyl-1H-indazol-4-ol

Suppliers and Price of 3-methyl-4,5,6,7-tetrahydro-1H-indazol-4-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3-methyl-4,5,6,7-tetrahydro-1H-indazol-4-ol

Chemical Property:

Melting Point:158-160 °C (isopropanol)
Boiling Point:379.6±37.0 °C (760 mmHg)
PSA：48.91000
Density:1.257±0.06 g/cm3 (20 °C, 760 mmHg)
LogP:1.08780
XLogP3:0.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:152.094963011
Heavy Atom Count:11
Complexity:151

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C2C(CCCC2=NN1)O

Technology Process of 3-methyl-4,5,6,7-tetrahydro-1H-indazol-4-ol

There total 2 articles about 3-methyl-4,5,6,7-tetrahydro-1H-indazol-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 63446-38-8
3-methyl-1,5,6,7-tetrahydro-4H-indazol-4-one

: 96546-41-7
3-Methyl-4,5,6,7-tetrahydro-1H-indazol-4-ol

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 40 ℃; for 4h;
DOI:10.1055/s-1984-31048

Reference yield:

: 4056-73-9
2-acetyl-1,3-cyclohexanedione

: 96546-41-7
3-Methyl-4,5,6,7-tetrahydro-1H-indazol-4-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NH₂-NH₂ / ethanol / 4 h / Ambient temperature

2: 80 percent / NaBH₄ / ethanol / 4 h / 40 °C

With sodium tetrahydroborate; hydrazine; In ethanol;
DOI:10.1055/s-1984-31048