(C₆H₅)2C₃H₃C₂H₄OHC₆H₄C₆H₃

Base Information

Chemical Name:(C₆H₅)2C₃H₃C₂H₄OHC₆H₄C₆H₃
CAS No.:478814-66-3
Molecular Formula:C₂₉H₂₅O
Molecular Weight:389.517
Hs Code.:

(C<sub>6</sub>H<sub>5</sub>)2C<sub>3</sub>H<sub>3</sub>C<sub>2</sub>H<sub>4</sub>OHC<sub>6</sub>H<sub>4</sub>C<sub>6</sub>H<sub>3</sub>

Synonyms:(C₆H₅)2C₃H₃C₂H₄OHC₆H₄C₆H₃

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Chemical Property of (C₆H₅)2C₃H₃C₂H₄OHC₆H₄C₆H₃

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Technology Process of (C₆H₅)2C₃H₃C₂H₄OHC₆H₄C₆H₃

There total 7 articles about (C₆H₅)2C₃H₃C₂H₄OHC₆H₄C₆H₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 478814-62-9
2-(2,2-diphenylcyclopropyl)-1,1-diphenylethyl 4-nitrobenzenesulfenate

: 478814-66-3
(C₆H₅)2C₃H₃C₂H₄OHC₆H₄C₆H₃

Guidance literature:: In acetonitrile; at 22 ℃; Photolysis;
DOI:10.1021/jo026218g

Reference yield:

: 7150-12-1
2,2-diphenyl-cyclopropanecarboxylic acid

: 478814-66-3
(C₆H₅)2C₃H₃C₂H₄OHC₆H₄C₆H₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: 98 percent / LiAlH₄ / diethyl ether / 0.75 h / 20 °C

2.1: 92 percent / PCC / CH₂Cl₂ / 2.5 h / 20 °C

3.1: lithium bis(trimethylsilyl)amide / tetrahydrofuran / 20 °C

3.2: 79 percent / HCl / tetrahydrofuran; H₂O / 2.5 h / Heating

4.1: 92 percent / Jones reagent / acetone / 0.17 h / 0 °C

5.1: 95 percent / p-toluenesulfonic acid / 1.5 h / Heating

6.1: 90 percent / tetrahydrofuran / 0.17 h / 20 °C

7.1: 75 percent / Et₃N / CH₂Cl₂ / 0.42 h / 0 - 20 °C

8.1: acetonitrile / 22 °C / Photolysis

With lithium aluminium tetrahydride; jones reagent; toluene-4-sulfonic acid; triethylamine; pyridinium chlorochromate; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; acetonitrile;
DOI:10.1021/jo026218g

Reference yield:

: 59591-01-4
2,2-diphenylcyclopropanecarbaldehyde

: 478814-66-3
(C₆H₅)2C₃H₃C₂H₄OHC₆H₄C₆H₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium bis(trimethylsilyl)amide / tetrahydrofuran / 20 °C

1.2: 79 percent / HCl / tetrahydrofuran; H₂O / 2.5 h / Heating

2.1: 92 percent / Jones reagent / acetone / 0.17 h / 0 °C

3.1: 95 percent / p-toluenesulfonic acid / 1.5 h / Heating

4.1: 90 percent / tetrahydrofuran / 0.17 h / 20 °C

5.1: 75 percent / Et₃N / CH₂Cl₂ / 0.42 h / 0 - 20 °C

6.1: acetonitrile / 22 °C / Photolysis

With jones reagent; toluene-4-sulfonic acid; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; acetone; acetonitrile;
DOI:10.1021/jo026218g