4-(4-acetylaminophenyl)-1,2-dihydro-2-(N,N-dimethylcarbamoyl)-1-methyl-6,7-methylendioxyphthalazine

Base Information

Chemical Name:4-(4-acetylaminophenyl)-1,2-dihydro-2-(N,N-dimethylcarbamoyl)-1-methyl-6,7-methylendioxyphthalazine
CAS No.:186252-78-8
Molecular Formula:C₂₁H₂₂N₄O₄
Molecular Weight:394.43
Hs Code.:

Synonyms:4-(4-acetylaminophenyl)-1,2-dihydro-2-(N,N-dimethylcarbamoyl)-1-methyl-6,7-methylendioxyphthalazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(4-acetylaminophenyl)-1,2-dihydro-2-(N,N-dimethylcarbamoyl)-1-methyl-6,7-methylendioxyphthalazine

Chemical Property:

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Technology Process of 4-(4-acetylaminophenyl)-1,2-dihydro-2-(N,N-dimethylcarbamoyl)-1-methyl-6,7-methylendioxyphthalazine

There total 3 articles about 4-(4-acetylaminophenyl)-1,2-dihydro-2-(N,N-dimethylcarbamoyl)-1-methyl-6,7-methylendioxyphthalazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 173952-39-1
4-(4-acetylaminophenyl)-1,2-dihydro-1-methyl-6,7-methylenedioxyphthalazine

: 79-44-7
N,N-Dimethylcarbamoyl chloride

: 186252-78-8
4-(4-acetylaminophenyl)-1,2-dihydro-2-(N,N-dimethylcarbamoyl)-1-methyl-6,7-methylendioxyphthalazine

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;

Reference yield:

: 173952-37-9
1-(4-aminophenyl)-6,7-methylenedioxyphthalazine

: 186252-78-8
4-(4-acetylaminophenyl)-1,2-dihydro-2-(N,N-dimethylcarbamoyl)-1-methyl-6,7-methylendioxyphthalazine

Guidance literature:: Multi-step reaction with 3 steps

1: acetic anhydride / hydrogenchloride

2: N,N,N,N,-tetramethylethylenediamine; methyllithium / tetrahydrofuran; methanol; dichloromethane; water

3: dmap; N-ethyl-N,N-diisopropylamine / tetrahydrofuran

With dmap; N,N,N,N,-tetramethylethylenediamine; methyllithium; acetic anhydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hydrogenchloride; methanol; dichloromethane; water;

Reference yield:

: 173952-38-0
1-(4-acetylaminophenyl)-6,7-methylenedioxyphthalazine

: 186252-78-8
4-(4-acetylaminophenyl)-1,2-dihydro-2-(N,N-dimethylcarbamoyl)-1-methyl-6,7-methylendioxyphthalazine

Guidance literature:: Multi-step reaction with 2 steps

1: N,N,N,N,-tetramethylethylenediamine; methyllithium / tetrahydrofuran; methanol; dichloromethane; water

2: dmap; N-ethyl-N,N-diisopropylamine / tetrahydrofuran

With dmap; N,N,N,N,-tetramethylethylenediamine; methyllithium; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water;