4-(4-acetylaminophenyl)-1,2-dihydro-1-methyl-6,7-methylenedioxyphthalazine

Base Information

Chemical Name:4-(4-acetylaminophenyl)-1,2-dihydro-1-methyl-6,7-methylenedioxyphthalazine
CAS No.:173952-39-1
Molecular Formula:C₁₈H₁₇N₃O₃
Molecular Weight:323.351
Hs Code.:

Synonyms:4-(4-acetylaminophenyl)-1,2-dihydro-1-methyl-6,7-methylenedioxyphthalazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(4-acetylaminophenyl)-1,2-dihydro-1-methyl-6,7-methylenedioxyphthalazine

Chemical Property:

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Technology Process of 4-(4-acetylaminophenyl)-1,2-dihydro-1-methyl-6,7-methylenedioxyphthalazine

There total 6 articles about 4-(4-acetylaminophenyl)-1,2-dihydro-1-methyl-6,7-methylenedioxyphthalazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 173952-38-0
1-(4-acetylaminophenyl)-6,7-methylenedioxyphthalazine

: 173952-39-1
4-(4-acetylaminophenyl)-1,2-dihydro-1-methyl-6,7-methylenedioxyphthalazine

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; methyllithium; In tetrahydrofuran; methanol; dichloromethane; water;

Reference yield:

: 173952-37-9
1-(4-aminophenyl)-6,7-methylenedioxyphthalazine

: 173952-39-1
4-(4-acetylaminophenyl)-1,2-dihydro-1-methyl-6,7-methylenedioxyphthalazine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 3 h / 20 °C

2: TMEDA / tetrahydrofuran

With N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran;
DOI:10.1021/jm950740w

Reference yield:

: 2139-43-7
5-bromo-6-(1,3-dioxolan-2-yl)benzo[d][1,3]dioxolane

: 173952-39-1
4-(4-acetylaminophenyl)-1,2-dihydro-1-methyl-6,7-methylenedioxyphthalazine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-BuLi / 1.) THF, -78 deg C, 2 min, 2.) THF

2: 94 percent / H₂NNH₂*HCl / methanol; H₂O

3: 85 percent / 3 h / 20 °C

4: TMEDA / tetrahydrofuran

With n-butyllithium; hydrazine hydrochloride; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; methanol; water;
DOI:10.1021/jm950740w