N¹,N¹²-diethyl-6-phthalimido-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

Base Information

Chemical Name:N¹,N¹²-diethyl-6-phthalimido-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine
CAS No.:852057-87-5
Molecular Formula:C₅₈H₇₇N₅O₁₀S₄
Molecular Weight:1132.54
Hs Code.:

N<sup>1</sup>,N<sup>12</sup>-diethyl-6-phthalimido-N<sup>1</sup>,N<sup>4</sup>,N<sup>9</sup>,N<sup>12</sup>-tetrakis(mesitylenesulfonyl)spermine

Synonyms:N¹,N¹²-diethyl-6-phthalimido-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹,N¹²-diethyl-6-phthalimido-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

Chemical Property:

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Technology Process of N¹,N¹²-diethyl-6-phthalimido-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

There total 3 articles about N¹,N¹²-diethyl-6-phthalimido-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 852057-86-4
N¹,N¹²-diethyl-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)-6-(p-toluenesulfonato)spermine

: 1074-82-4
potassium phtalimide

: 852057-87-5
N¹,N¹²-diethyl-6-phthalimido-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

Guidance literature:: In N,N-dimethyl-formamide; at 85 ℃; for 18h;
DOI:10.1021/jm050024m

Reference yield:

: 852057-85-3
N¹,N¹²-diethyl-6-hydroxy-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

: 852057-87-5
N¹,N¹²-diethyl-6-phthalimido-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / pyridine / CH₂Cl₂ / 24 h / 20 °C

2: 62 percent / dimethylformamide / 18 h / 85 °C

With pyridine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm050024m

Reference yield:

: 206991-72-2
N,N'-bis(mesitylenesulfonyl)-N-ethyl-1,3-diaminopropane

: 852057-87-5
N¹,N¹²-diethyl-6-phthalimido-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / dimethylformamide / 0.5 h

1.2: 80 percent / dimethylformamide / 18 h / 70 °C

2.1: 61 percent / pyridine / CH₂Cl₂ / 24 h / 20 °C

3.1: 62 percent / dimethylformamide / 18 h / 85 °C

With pyridine; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm050024m