Benzaldehyde (3-benzyl-5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone

Base Information

Chemical Name:Benzaldehyde (3-benzyl-5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone
CAS No.:216085-06-2
Molecular Formula:C₂₅H₁₉N₅O
Molecular Weight:405.459
Hs Code.:

Synonyms:Benzaldehyde (3-benzyl-5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzaldehyde (3-benzyl-5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone

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Technology Process of Benzaldehyde (3-benzyl-5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone

There total 3 articles about Benzaldehyde (3-benzyl-5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 100-52-7
benzaldehyde

: 216084-77-4
3-Benzyl-5-cyano-2-hydrazino-6-phenyl-3,4-dihydropyrimidin-4-one

: 216085-06-2
Benzaldehyde (3-benzyl-5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone

Guidance literature:: With acetic acid; In ethanol; for 1h; Heating;
DOI:10.1515/znb-1998-1017

Reference yield:

: 1,6-dihydro-2-mercapto-6-oxo-4-phenylpyrimidine-5-carbonitrile

: 216085-06-2
Benzaldehyde (3-benzyl-5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 46 percent / KOH / dimethylformamide / 4 h / Heating

2: 80 percent / N₂H₄*H₂O / ethanol / 1 h / Heating

3: 73 percent / AcOH / ethanol / 1 h / Heating

With potassium hydroxide; hydrazine hydrate; acetic acid; In ethanol; N,N-dimethyl-formamide;
DOI:10.1515/znb-1998-1017

Reference yield:

: 216084-76-3
3-Benzyl-2-benzylthio-5-cyano-6-phenyl-3,4-dihydropyrimidin-4-one

: 216085-06-2
Benzaldehyde (3-benzyl-5-cyano-4-oxo-6-phenyl-3,4-dihydropyrimidin-2-yl)hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / N₂H₄*H₂O / ethanol / 1 h / Heating

2: 73 percent / AcOH / ethanol / 1 h / Heating

With hydrazine hydrate; acetic acid; In ethanol;
DOI:10.1515/znb-1998-1017