dibutyl[5,10-dihydro-1,9-bis(4-methylbenzoyl)-5-phenyldipyrrinato]tin(IV)

Base Information

• Chemical Name: dibutyl[5,10-dihydro-1,9-bis(4-methylbenzoyl)-5-phenyldipyrrinato]tin(IV)
• CAS No.: 816454-44-1
• Molecular Formula: C₃₉H₄₂N₂O₂Sn
• Molecular Weight: 689.485
• Mol file: 816454-44-1.mol

Synonyms:dibutyl[5,10-dihydro-1,9-bis(4-methylbenzoyl)-5-phenyldipyrrinato]tin(IV)

Chemical Property of dibutyl[5,10-dihydro-1,9-bis(4-methylbenzoyl)-5-phenyldipyrrinato]tin(IV)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dibutyl[5,10-dihydro-1,9-bis(4-methylbenzoyl)-5-phenyldipyrrinato]tin(IV)

There total 4 articles about dibutyl[5,10-dihydro-1,9-bis(4-methylbenzoyl)-5-phenyldipyrrinato]tin(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

dibutyltin chloride (683-18-1) + 1,9-bis-(4-methylbenzoyl)-5-phenyldipyrromethane (171523-04-9) → dibutyl[5,10-dihydro-1,9-bis(4-methylbenzoyl)-5-phenyldipyrrinato]tin(IV) (816454-44-1)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield: 66.0%

dibutyltin chloride (683-18-1) + 4-methyl-benzoyl chloride (874-60-2) + 1-(p-methylbenzoyl)-5-phenyldipyrromethane (171523-03-8) → dibutyl[5,10-dihydro-1,9-bis(4-methylbenzoyl)-5-phenyldipyrrinato]tin(IV) (816454-44-1) + (5-{[4-(4-methyl-benzoyl)-1H-pyrrol-2-yl]-phenyl-methyl}-1H-pyrrol-2-yl)-p-tolyl-methanone

Guidance literature:

4-methyl-benzoyl chloride; 1-(p-methylbenzoyl)-5-phenyldipyrromethane; antimonypentachloride; In dichloromethane; at 20 ℃; for 0.166667h;

dibutyltin chloride; With triethylamine; In dichloromethane; at 20 ℃; for 0.25h;

Reference yield: 60.0%

dibutyltin chloride (683-18-1) + 4-methyl-benzoyl chloride (874-60-2) + 1-(p-methylbenzoyl)-5-phenyldipyrromethane (171523-03-8) → dibutyl[5,10-dihydro-1,9-bis(4-methylbenzoyl)-5-phenyldipyrrinato]tin(IV) (816454-44-1)

Guidance literature:

4-methyl-benzoyl chloride; 1-(p-methylbenzoyl)-5-phenyldipyrromethane; tin(IV) chloride; In 1,2-dichloro-ethane; at 20 ℃; for 0.166667h;

dibutyltin chloride; With triethylamine; In dichloromethane; at 20 ℃; for 0.25h;

upstream raw materials:

dibutyltin chloride

1,9-bis-(4-methylbenzoyl)-5-phenyldipyrromethane

4-methyl-benzoyl chloride

5-phenyldipyrromethane

Downstream raw materials:

1,9-bis[α-hydroxy-α-(p-tolyl)methyl]-5-phenyldipyrromethane

1,9-bis-(4-methylbenzoyl)-5-phenyldipyrromethane