2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid

Base Information

• Chemical Name: 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid
• CAS No.: 1383577-47-6
• Molecular Formula: C₁₇H₁₄N₄O₄
• Molecular Weight: 338.323

Synonyms:2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid

Chemical Property of 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid

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Technology Process of 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid

There total 1 articles about 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2-azidobenzoic acid (31162-13-7) + propargyl anthranilate (90923-99-2) → 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid (1383577-47-6)

Guidance literature:

With copper(II) sulfate; ascorbic acid; In water; butan-1-ol; at 20 ℃; for 1h;

DOI:10.1055/s-0031-1290760

Reference yield: 93.0%

2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid (1383577-47-6) → 2-(4-([(2-azidophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid (1383577-51-2)

Guidance literature:

2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid; With hydrogenchloride; In water; acetone;

With sodium nitrite; In water; acetone; at 0 ℃; for 0.0833333h;

With sodium azide; In water; acetone; at 0 - 20 ℃; for 0.5h;

DOI:10.1055/s-0031-1290760

Reference yield: 84.0%

2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid (1383577-47-6) + propargyl bromide (106-96-7) → prop-2-yn-1-yl 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate (1383577-49-8)

Guidance literature:

2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid; With potassium carbonate; In N,N-dimethyl-formamide; for 0.0833333h; Reflux;

propargyl bromide; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1055/s-0031-1290760

upstream raw materials:

2-azidobenzoic acid

propargyl anthranilate

Downstream raw materials:

2-(4-([(2-azidophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid

2-[4-(([2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)phenyl]carbonyloxy)methyl)-1H-1,2,3-triazol-1-yl]benzoic acid

(1-{2-[(prop-2-yn-1-yloxy)carbonyl]phenyl}-1H-1,2,3-triazol-4-yl)methyl 2-(4-{[(2-aminophenyl)carbonyloxy]methyl}-1H-1,2,3-triazol-1-yl)benzoate

2-(4-[((2-[4-(([2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)phenyl]carbonyloxy)methyl)-1H-1,2,3-triazol-1-yl]phenyl)carbonyloxy)methyl]-1H-1,2,3-triazol-1-yl)benzoic acid

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