(1-{2-[(prop-2-yn-1-yloxy)carbonyl]phenyl}-1H-1,2,3-triazol-4-yl)methyl 2-(4-{[(2-aminophenyl)carbonyloxy]methyl}-1H-1,2,3-triazol-1-yl)benzoate

Base Information

Chemical Name:(1-{2-[(prop-2-yn-1-yloxy)carbonyl]phenyl}-1H-1,2,3-triazol-4-yl)methyl 2-(4-{[(2-aminophenyl)carbonyloxy]methyl}-1H-1,2,3-triazol-1-yl)benzoate
CAS No.:1383577-53-4
Molecular Formula:C₃₀H₂₃N₇O₆
Molecular Weight:577.556
Hs Code.:

Synonyms:(1-{2-[(prop-2-yn-1-yloxy)carbonyl]phenyl}-1H-1,2,3-triazol-4-yl)methyl 2-(4-{[(2-aminophenyl)carbonyloxy]methyl}-1H-1,2,3-triazol-1-yl)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1-{2-[(prop-2-yn-1-yloxy)carbonyl]phenyl}-1H-1,2,3-triazol-4-yl)methyl 2-(4-{[(2-aminophenyl)carbonyloxy]methyl}-1H-1,2,3-triazol-1-yl)benzoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (1-{2-[(prop-2-yn-1-yloxy)carbonyl]phenyl}-1H-1,2,3-triazol-4-yl)methyl 2-(4-{[(2-aminophenyl)carbonyloxy]methyl}-1H-1,2,3-triazol-1-yl)benzoate

There total 5 articles about (1-{2-[(prop-2-yn-1-yloxy)carbonyl]phenyl}-1H-1,2,3-triazol-4-yl)methyl 2-(4-{[(2-aminophenyl)carbonyloxy]methyl}-1H-1,2,3-triazol-1-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1383577-52-3
2-[4-(([2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)phenyl]carbonyloxy)methyl)-1H-1,2,3-triazol-1-yl]benzoic acid

: 106-96-7
propargyl bromide

: 1383577-53-4
(1-{2-[(prop-2-yn-1-yloxy)carbonyl]phenyl}-1H-1,2,3-triazol-4-yl)methyl 2-(4-{[(2-aminophenyl)carbonyloxy]methyl}-1H-1,2,3-triazol-1-yl)benzoate

Guidance literature:: 2-[4-(([2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)phenyl]carbonyloxy)methyl)-1H-1,2,3-triazol-1-yl]benzoic acid; With potassium carbonate; In N,N-dimethyl-formamide; for 0.0833333h; Reflux;

propargyl bromide; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1055/s-0031-1290760

Reference yield:

: 90923-99-2
propargyl anthranilate

: 1383577-53-4
(1-{2-[(prop-2-yn-1-yloxy)carbonyl]phenyl}-1H-1,2,3-triazol-4-yl)methyl 2-(4-{[(2-aminophenyl)carbonyloxy]methyl}-1H-1,2,3-triazol-1-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(II) sulfate; ascorbic acid / water; N,N-dimethyl-formamide / 0.5 h / 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.08 h / Reflux

2.2: 20 °C

With potassium carbonate; copper(II) sulfate; ascorbic acid; In water; N,N-dimethyl-formamide;
DOI:10.1055/s-0031-1290760

Reference yield:

: 1383577-51-2
2-(4-([(2-azidophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid

: 1383577-53-4
(1-{2-[(prop-2-yn-1-yloxy)carbonyl]phenyl}-1H-1,2,3-triazol-4-yl)methyl 2-(4-{[(2-aminophenyl)carbonyloxy]methyl}-1H-1,2,3-triazol-1-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(II) sulfate; ascorbic acid / water; N,N-dimethyl-formamide / 0.5 h / 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.08 h / Reflux

2.2: 20 °C

With potassium carbonate; copper(II) sulfate; ascorbic acid; In water; N,N-dimethyl-formamide;
DOI:10.1055/s-0031-1290760