benzyl(6-bromohexyl)sulfane

Base Information

Chemical Name:benzyl(6-bromohexyl)sulfane
CAS No.:93043-39-1
Molecular Formula:C₁₃H₁₉BrS
Molecular Weight:287.264
Hs Code.:

Synonyms:benzyl(6-bromohexyl)sulfane

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Chemical Property of benzyl(6-bromohexyl)sulfane

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Technology Process of benzyl(6-bromohexyl)sulfane

There total 2 articles about benzyl(6-bromohexyl)sulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 2695-47-8
6-Bromo-1-hexene

: 100-53-8
phenylmethanethiol

: 93043-39-1
benzyl(6-bromohexyl)sulfane

Guidance literature:: With tris(2-carboxyethyl)phosphine; [Gd(ADBEB)(DMF)(HCOO)]; In N,N-dimethyl-formamide; acetonitrile; at 25 ℃; for 8h; Inert atmosphere; Irradiation;
DOI:10.1021/acs.inorgchem.1c00642

Reference yield:

: 150-60-7
dibenzyl disulphide

: 93043-39-1
benzyl(6-bromohexyl)sulfane

Guidance literature:: Multi-step reaction with 2 steps

1: tris(2-carboxyethyl)phosphine / N,N-dimethyl-formamide; acetonitrile / 5 h / Darkness; Inert atmosphere

2: [Gd(ADBEB)(DMF)(HCOO)]; tris(2-carboxyethyl)phosphine / N,N-dimethyl-formamide; acetonitrile / 8 h / 25 °C / Inert atmosphere; Irradiation

With tris(2-carboxyethyl)phosphine; [Gd(ADBEB)(DMF)(HCOO)]; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/acs.inorgchem.1c00642