methyl [tert-butyl (2-O-benzoyl-3,4-di-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-[tert-butyl (2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

Base Information

• Chemical Name: methyl [tert-butyl (2-O-benzoyl-3,4-di-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-[tert-butyl (2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)
• CAS No.: 1253183-83-3
• Molecular Formula: C₉₈H₁₀₈N₄O₂₄
• Molecular Weight: 1725.95

Synonyms:methyl [tert-butyl (2-O-benzoyl-3,4-di-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-[tert-butyl (2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

Chemical Property of methyl [tert-butyl (2-O-benzoyl-3,4-di-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-[tert-butyl (2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of methyl [tert-butyl (2-O-benzoyl-3,4-di-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-[tert-butyl (2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

There total 2 articles about methyl [tert-butyl (2-O-benzoyl-3,4-di-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-[tert-butyl (2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

methyl [tert-butyl (2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside) (1253183-73-1) + phenyl [tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside) (1253183-67-3) → methyl [tert-butyl (2-O-benzoyl-3,4-di-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-[tert-butyl (2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside) (1253183-83-3)

Guidance literature:

With 2,6-di-tert-butyl-4-methylpyridine; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In diethyl ether; dichloromethane; at 0 - 20 ℃; for 48h; stereoselective reaction; Molecular sieve; Inert atmosphere;

DOI:10.1016/j.tet.2010.08.004

Reference yield: 53.0%

methyl [tert-butyl (2-O-benzoyl-3,4-di-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-(2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl)-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside) (1253183-81-1) + tert-butyl alcohol (75-65-0) → methyl [tert-butyl (2-O-benzoyl-3,4-di-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-[tert-butyl (2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside) (1253183-83-3)

Guidance literature:

With dipyridinium dichromate; acetic anhydride; In dichloromethane; at 20 ℃;

DOI:10.1016/j.tet.2010.08.004

Reference yield: 64.0%

methyl [tert-butyl (2-O-benzoyl-3,4-di-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-[tert-butyl (2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside) (1253183-83-3) → C84H100N4O22 (1253183-87-7)

Guidance literature:

With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 72h;

DOI:10.1016/j.tet.2010.08.004

upstream raw materials:

methyl [tert-butyl (2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

phenyl [tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside)

methyl [tert-butyl (2-O-benzoyl-3,4-di-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-(2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl)-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

tert-butyl alcohol

Downstream raw materials:

C₈₄H₁₀₀N₄O₂₂

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