9-(carbophenoxy)-9-azabicyclo<3.3.1>nonane-2,6-dione bis(2,2-dimethylpropylene) ketal

Base Information

Chemical Name:9-(carbophenoxy)-9-azabicyclo<3.3.1>nonane-2,6-dione bis(2,2-dimethylpropylene) ketal
CAS No.:80627-95-8
Molecular Formula:C₂₅H₃₅NO₆
Molecular Weight:445.556
Hs Code.:

Synonyms:9-(carbophenoxy)-9-azabicyclo<3.3.1>nonane-2,6-dione bis(2,2-dimethylpropylene) ketal

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Chemical Property of 9-(carbophenoxy)-9-azabicyclo<3.3.1>nonane-2,6-dione bis(2,2-dimethylpropylene) ketal

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Technology Process of 9-(carbophenoxy)-9-azabicyclo<3.3.1>nonane-2,6-dione bis(2,2-dimethylpropylene) ketal

There total 5 articles about 9-(carbophenoxy)-9-azabicyclo<3.3.1>nonane-2,6-dione bis(2,2-dimethylpropylene) ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 80627-99-2
9-(carbophenoxy)-2,6-dioxo-9-azabicyclo<3.3.1>nonane-2,6-dione

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 80627-95-8
9-(carbophenoxy)-9-azabicyclo<3.3.1>nonane-2,6-dione bis(2,2-dimethylpropylene) ketal

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 3.25h; Heating;
DOI:10.1021/jo00345a004

Reference yield:

: 57639-00-6
N-methyl-2,6-diacetoxy-9-azabicyclo<3.3.1>nonane

: 80627-95-8
9-(carbophenoxy)-9-azabicyclo<3.3.1>nonane-2,6-dione bis(2,2-dimethylpropylene) ketal

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / LiI / acetone / 1.) 0 deg C, 2.) 25 deg C, 3.5 h

2: 98 percent / K₂CO₃ / methanol; H₂O / 2 h / Ambient temperature

3: 56.4 percent / pyridinium chlorochromate (PCC) / CHCl₃ / 26 h / 25 °C

4: 86 percent / p-toluenesulfonic acid monohydrate / toluene / 3.25 h / Heating

With potassium carbonate; toluene-4-sulfonic acid; pyridinium chlorochromate; lithium iodide; In methanol; chloroform; water; acetone; toluene;
DOI:10.1021/jo00345a004

Reference yield:

: 80628-00-8
9-(carbophenoxy)-endo,endo-2,6-dihydroxy-9-azabicyclo<3.3.1>nonane

: 80627-95-8
9-(carbophenoxy)-9-azabicyclo<3.3.1>nonane-2,6-dione bis(2,2-dimethylpropylene) ketal

Guidance literature:: Multi-step reaction with 2 steps

1: 56.4 percent / pyridinium chlorochromate (PCC) / CHCl₃ / 26 h / 25 °C

2: 86 percent / p-toluenesulfonic acid monohydrate / toluene / 3.25 h / Heating

With toluene-4-sulfonic acid; pyridinium chlorochromate; In chloroform; toluene;
DOI:10.1021/jo00345a004