5-ethoxy-6-methyl-6-(4-methylphenyl)-3,6-dihydro-2H-1,3,4-oxadiazin-2-one

Base Information

Chemical Name:5-ethoxy-6-methyl-6-(4-methylphenyl)-3,6-dihydro-2H-1,3,4-oxadiazin-2-one
CAS No.:1373618-09-7
Molecular Formula:C₁₃H₁₆N₂O₃
Molecular Weight:248.282
Hs Code.:

Synonyms:5-ethoxy-6-methyl-6-(4-methylphenyl)-3,6-dihydro-2H-1,3,4-oxadiazin-2-one

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Chemical Property of 5-ethoxy-6-methyl-6-(4-methylphenyl)-3,6-dihydro-2H-1,3,4-oxadiazin-2-one

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Technology Process of 5-ethoxy-6-methyl-6-(4-methylphenyl)-3,6-dihydro-2H-1,3,4-oxadiazin-2-one

There total 4 articles about 5-ethoxy-6-methyl-6-(4-methylphenyl)-3,6-dihydro-2H-1,3,4-oxadiazin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: C₁₅H₂₂N₂O₄

: 1373618-09-7
5-ethoxy-6-methyl-6-(4-methylphenyl)-3,6-dihydro-2H-1,3,4-oxadiazin-2-one

Guidance literature:: With sodium ethanolate; In ethanol; at 100 ℃; for 0.0833333h; under 7500.75 Torr; Microwave irradiation;
DOI:10.1055/s-0031-1290160

Reference yield:

: 1352808-52-6
O-ethyl 2-hydroxy-2-(4-methylphenyl)propanethioate

: 1373618-09-7
5-ethoxy-6-methyl-6-(4-methylphenyl)-3,6-dihydro-2H-1,3,4-oxadiazin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: ethyl acetate / 20 °C

2: sodium ethanolate / ethanol / 0.08 h / 100 °C / 7500.75 Torr / Microwave irradiation

With sodium ethanolate; In ethanol; ethyl acetate;
DOI:10.1055/s-0031-1290160

Reference yield:

: 69813-74-7
2-hydroxy-2-methyl-2-(4'-methylphenyl)acetonitrile

: 1373618-09-7
5-ethoxy-6-methyl-6-(4-methylphenyl)-3,6-dihydro-2H-1,3,4-oxadiazin-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / diethyl ether / 0 °C

2: pyridine; hydrogen sulfide / dichloromethane / 5 - 20 °C

3: ethyl acetate / 20 °C

4: sodium ethanolate / ethanol / 0.08 h / 100 °C / 7500.75 Torr / Microwave irradiation

With pyridine; hydrogenchloride; hydrogen sulfide; sodium ethanolate; In diethyl ether; ethanol; dichloromethane; ethyl acetate; 1: Pinner amidine synthesis;
DOI:10.1055/s-0031-1290160