Technology Process of 5-ethoxy-6-methyl-6-(4-methylphenyl)-3,6-dihydro-2H-1,3,4-oxadiazin-2-one
There total 4 articles about 5-ethoxy-6-methyl-6-(4-methylphenyl)-3,6-dihydro-2H-1,3,4-oxadiazin-2-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium ethanolate;
In
ethanol;
at 100 ℃;
for 0.0833333h;
under 7500.75 Torr;
Microwave irradiation;
DOI:10.1055/s-0031-1290160
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ethyl acetate / 20 °C
2: sodium ethanolate / ethanol / 0.08 h / 100 °C / 7500.75 Torr / Microwave irradiation
With
sodium ethanolate;
In
ethanol; ethyl acetate;
DOI:10.1055/s-0031-1290160
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride / diethyl ether / 0 °C
2: pyridine; hydrogen sulfide / dichloromethane / 5 - 20 °C
3: ethyl acetate / 20 °C
4: sodium ethanolate / ethanol / 0.08 h / 100 °C / 7500.75 Torr / Microwave irradiation
With
pyridine; hydrogenchloride; hydrogen sulfide; sodium ethanolate;
In
diethyl ether; ethanol; dichloromethane; ethyl acetate;
1: Pinner amidine synthesis;
DOI:10.1055/s-0031-1290160
