2-[4-(3-allyloxy-phenyl)butyl]-4,6-dimethyl-pyrimidine-5-carboxylic acid methyl ester

Base Information

Chemical Name:2-[4-(3-allyloxy-phenyl)butyl]-4,6-dimethyl-pyrimidine-5-carboxylic acid methyl ester
CAS No.:1400705-51-2
Molecular Formula:C₂₁H₂₆N₂O₃
Molecular Weight:354.449
Hs Code.:

Synonyms:2-[4-(3-allyloxy-phenyl)butyl]-4,6-dimethyl-pyrimidine-5-carboxylic acid methyl ester

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Chemical Property of 2-[4-(3-allyloxy-phenyl)butyl]-4,6-dimethyl-pyrimidine-5-carboxylic acid methyl ester

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Technology Process of 2-[4-(3-allyloxy-phenyl)butyl]-4,6-dimethyl-pyrimidine-5-carboxylic acid methyl ester

There total 6 articles about 2-[4-(3-allyloxy-phenyl)butyl]-4,6-dimethyl-pyrimidine-5-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1400706-25-3
C₁₄H₂₀N₂O

: 80751-03-7
2-acetyl-3-methoxy-but-2-enoic acid methyl ester

: 1400705-51-2
2-[4-(3-allyloxy-phenyl)butyl]-4,6-dimethyl-pyrimidine-5-carboxylic acid methyl ester

Guidance literature:: With pyridine; acetic acid; In methanol; for 26h; Reflux;

Reference yield:

: 626-02-8
3-Iodophenol

: 1400705-51-2
2-[4-(3-allyloxy-phenyl)butyl]-4,6-dimethyl-pyrimidine-5-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate; tetrabutyl-ammonium chloride / palladium diacetate / N,N-dimethyl-formamide / 1 h / 70 °C

1.2: 20 °C

2.1: hydrogen / palladium 10% on activated carbon / methanol / 2585.81 Torr

3.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 60 °C

4.1: Lawessons reagent / xylenes / 3 h / Reflux

5.1: ammonia; ammonium chloride / methanol / 0.67 h / Reflux

6.1: pyridine; acetic acid / methanol / 26 h / Reflux

With Lawessons reagent; pyridine; tetrabutyl-ammonium chloride; ammonia; hydrogen; potassium carbonate; ammonium chloride; acetic acid; palladium 10% on activated carbon; palladium diacetate; In methanol; N,N-dimethyl-formamide; xylenes;

Reference yield:

: 1400705-30-7
5-(3-hydroxy-phenyl)-4-pentenoic acid ethyl ester

: 1400705-51-2
2-[4-(3-allyloxy-phenyl)butyl]-4,6-dimethyl-pyrimidine-5-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 2585.81 Torr

2: potassium carbonate / N,N-dimethyl-formamide / 12 h / 60 °C

3: Lawessons reagent / xylenes / 3 h / Reflux

4: ammonia; ammonium chloride / methanol / 0.67 h / Reflux

5: pyridine; acetic acid / methanol / 26 h / Reflux

With Lawessons reagent; pyridine; ammonia; hydrogen; potassium carbonate; ammonium chloride; acetic acid; palladium 10% on activated carbon; In methanol; N,N-dimethyl-formamide; xylenes;