2-(4-(1,3-dithian-2-yl)phenyl)-1H-phenanthro[9,10-d]imidazole

Base Information

• Chemical Name: 2-(4-(1,3-dithian-2-yl)phenyl)-1H-phenanthro[9,10-d]imidazole
• CAS No.: 1131797-24-4
• Molecular Formula: C₂₅H₂₀N₂S₂
• Molecular Weight: 412.579
• Mol file: 1131797-24-4.mol

Synonyms:2-(4-(1,3-dithian-2-yl)phenyl)-1H-phenanthro[9,10-d]imidazole

Chemical Property of 2-(4-(1,3-dithian-2-yl)phenyl)-1H-phenanthro[9,10-d]imidazole

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-(4-(1,3-dithian-2-yl)phenyl)-1H-phenanthro[9,10-d]imidazole

There total 1 articles about 2-(4-(1,3-dithian-2-yl)phenyl)-1H-phenanthro[9,10-d]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

1.3-propanedithiol (109-80-8) + 4-(1H-phenanthrol-[9,10-d]imidazole-2-yl)benzaldehyde (1092490-83-9) → 2-(4-(1,3-dithian-2-yl)phenyl)-1H-phenanthro[9,10-d]imidazole (1131797-24-4)

Guidance literature:

With boron trifluoride diethyl etherate; In N,N-dimethyl-formamide; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1002/chem.200801501

Reference yield:

2-(4-(1,3-dithian-2-yl)phenyl)-1H-phenanthro[9,10-d]imidazole (1131797-24-4) → 4-(1H-phenanthrol-[9,10-d]imidazole-2-yl)benzaldehyde (1092490-83-9)

Guidance literature:

With copper dichloride; In acetonitrile; at 20 ℃; for 0.416667h;

DOI:10.1002/chem.200801501

upstream raw materials:

1.3-propanedithiol

4-(1H-phenanthrol-[9,10-d]imidazole-2-yl)benzaldehyde

Downstream raw materials:

4-(1H-phenanthrol-[9,10-d]imidazole-2-yl)benzaldehyde