(1R,2R,3S,4S)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dimethyl biscarbonate

Base Information

Chemical Name:(1R*,2R*,3S*,4S*)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dimethyl biscarbonate
CAS No.:1226781-28-7
Molecular Formula:C₁₂H₁₆O₇
Molecular Weight:272.255
Hs Code.:

Synonyms:(1R*,2R*,3S*,4S*)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dimethyl biscarbonate

Suppliers and Price of (1R*,2R*,3S*,4S*)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dimethyl biscarbonate

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Chemical Property of (1R*,2R*,3S*,4S*)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dimethyl biscarbonate

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Technology Process of (1R*,2R*,3S*,4S*)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dimethyl biscarbonate

There total 1 articles about (1R*,2R*,3S*,4S*)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dimethyl biscarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6118-51-0
exo-3,6-epoxy-1,2,3,6-tetrahydrophthalic anhydride

: 1226781-28-7
(1R*,2R*,3S*,4S*)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dimethyl biscarbonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 24 h / -10 - 20 °C / Inert atmosphere

1.2: 16 h / 20 °C

2.1: dmap; pyridine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With pyridine; dmap; lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/adsc.201500971