Dibutyl-[4-((E)-2-{4-[(E)-2-(4-diethoxymethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine

Base Information

Chemical Name:Dibutyl-[4-((E)-2-{4-[(E)-2-(4-diethoxymethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine
CAS No.:854200-43-4
Molecular Formula:C₃₅H₄₅NO₂
Molecular Weight:511.748
Hs Code.:

Synonyms:Dibutyl-[4-((E)-2-{4-[(E)-2-(4-diethoxymethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine

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Chemical Property of Dibutyl-[4-((E)-2-{4-[(E)-2-(4-diethoxymethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine

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Technology Process of Dibutyl-[4-((E)-2-{4-[(E)-2-(4-diethoxymethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine

There total 3 articles about Dibutyl-[4-((E)-2-{4-[(E)-2-(4-diethoxymethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 160469-44-3
N,N-dibutyl-4-vinylbenzenamine

: 663933-31-1
C₆H₄C₂H₂IC₆H₄CH(OCH₂CH₃)2

: 854200-43-4
Dibutyl-[4-((E)-2-{4-[(E)-2-(4-diethoxymethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine

Guidance literature:: With triethylamine; tris-(o-tolyl)phosphine; palladium diacetate; In N,N-dimethyl-formamide; for 17h; Heating;
DOI:10.1016/j.tetlet.2003.10.099

Reference yield:

: 16004-15-2
1-bromomethyl-4-iodobenzene

: 854200-43-4
Dibutyl-[4-((E)-2-{4-[(E)-2-(4-diethoxymethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / 17 h / Heating

2: 98 percent / NaH / tetrahydrofuran / 3 h / Heating

3: 48 percent / P(o-tolyl)3; NEt₃ / Pd(OAc)2 / dimethylformamide / 17 h / Heating

With sodium hydride; triethylamine; tris-(o-tolyl)phosphine; palladium diacetate; In tetrahydrofuran; N,N-dimethyl-formamide; 3: Heck cross-coupling reaction;
DOI:10.1016/j.tetlet.2003.10.099

Reference yield:

: 173443-43-1
diethyl (4-iodobenzyl)phosphonate

: 854200-43-4
Dibutyl-[4-((E)-2-{4-[(E)-2-(4-diethoxymethyl-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NaH / tetrahydrofuran / 3 h / Heating

2: 48 percent / P(o-tolyl)3; NEt₃ / Pd(OAc)2 / dimethylformamide / 17 h / Heating

With sodium hydride; triethylamine; tris-(o-tolyl)phosphine; palladium diacetate; In tetrahydrofuran; N,N-dimethyl-formamide; 2: Heck cross-coupling reaction;
DOI:10.1016/j.tetlet.2003.10.099