(-)-[1R,(S)R]-1-iodo-6-methoxy-2-[1-methoxy-2-(p-tolylsulfinyl)ethyl]benzene

Base Information

• Chemical Name: (-)-[1R,(S)R]-1-iodo-6-methoxy-2-[1-methoxy-2-(p-tolylsulfinyl)ethyl]benzene
• CAS No.: 607356-05-8
• Molecular Formula: C₁₇H₁₉IO₃S
• Molecular Weight: 430.307

Synonyms:(-)-[1R,(S)R]-1-iodo-6-methoxy-2-[1-methoxy-2-(p-tolylsulfinyl)ethyl]benzene

Chemical Property of (-)-[1R,(S)R]-1-iodo-6-methoxy-2-[1-methoxy-2-(p-tolylsulfinyl)ethyl]benzene

Chemical Property:

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Technology Process of (-)-[1R,(S)R]-1-iodo-6-methoxy-2-[1-methoxy-2-(p-tolylsulfinyl)ethyl]benzene

There total 1 articles about (-)-[1R,(S)R]-1-iodo-6-methoxy-2-[1-methoxy-2-(p-tolylsulfinyl)ethyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-1-(2-Iodo-3-methoxy-phenyl)-2-((R)-toluene-4-sulfinyl)-ethanol + methyl iodide (74-88-4) → (-)-[1R,(S)R]-1-iodo-6-methoxy-2-[1-methoxy-2-(p-tolylsulfinyl)ethyl]benzene (607356-05-8)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at -20 ℃;

DOI:10.1021/ol0351908

Reference yield: 95.0%

2-(2-methoxyphenyl)-1,3,2-dioxaborolane (536744-01-1) + (-)-[1R,(S)R]-1-iodo-6-methoxy-2-[1-methoxy-2-(p-tolylsulfinyl)ethyl]benzene (607356-05-8) → [1R,(S)R]-2,2'-dimethoxy-6-[1-methoxy-2-(p-tolylsulfinyl)ethyl]biphenyl

Guidance literature:

With 1,1'-bis-(diphenylphosphino)ferrocene; cesium fluoride; palladium diacetate; In 1,4-dioxane; at 70 ℃; for 1h;

DOI:10.1002/ejoc.200400638

Reference yield: 86.0%

2-(naphthalen-1-yl)-1,3,2-dioxaborolane (402488-95-3) + (-)-[1R,(S)R]-1-iodo-6-methoxy-2-[1-methoxy-2-(p-tolylsulfinyl)ethyl]benzene (607356-05-8) → [1R,(S)R]-1-{2-methoxy-6-[1-methoxy-2-(p-tolylsulfinyl)ethyl]phenyl}naphthalene

Guidance literature:

With triphenylphosphine; cesium fluoride; palladium diacetate; In 1,4-dioxane; at 110 ℃;

DOI:10.1021/ol0351908

upstream raw materials:

methyl iodide

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