Octyl-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-(1->6)-2,4-di-O-benzyl-β-D-mannopyranosid

Base Information

Chemical Name:Octyl-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-(1->6)-2,4-di-O-benzyl-β-D-mannopyranosid
CAS No.:151413-76-2
Molecular Formula:C₄₂H₅₈O₁₅
Molecular Weight:802.914
Hs Code.:

Synonyms:Octyl-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-(1->6)-2,4-di-O-benzyl-β-D-mannopyranosid

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Chemical Property of Octyl-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-(1->6)-2,4-di-O-benzyl-β-D-mannopyranosid

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Technology Process of Octyl-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-(1->6)-2,4-di-O-benzyl-β-D-mannopyranosid

There total 5 articles about Octyl-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-(1->6)-2,4-di-O-benzyl-β-D-mannopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 121238-27-5
2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl trichloroimidate

: 141936-73-4
Octyl 2,4-di-O-benzyl-β-D-mannopyranoside

: 151413-76-2
Octyl-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-(1->6)-2,4-di-O-benzyl-β-D-mannopyranosid

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 3 A molecular sieve; In dichloromethane; for 2h; -20 deg C to r.t.;

Reference yield:

: 100-39-0
benzyl bromide

: 151413-76-2
Octyl-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-(1->6)-2,4-di-O-benzyl-β-D-mannopyranosid

Guidance literature:: Multi-step reaction with 3 steps

2: 77 percent / hydrogenated 1,5-cyclooctadiene-bis(methyldiphenylphosphine)iridium hexafluorophosphate / tetrahydrofuran / 2 h

3: 80 percent / molecular sieves 3 Angstroem, trimethylsilyl triflate / CH₂Cl₂ / 2 h / -20 deg C to r.t.

With trimethylsilyl trifluoromethanesulfonate; 3 A molecular sieve; hydrogenated 1,5-cyclooctadiene-bis(methyldiphenylphosphine)iridium hexafluorophosphate; In tetrahydrofuran; dichloromethane;

Reference yield:

: 139493-94-0
Octyl-3,6-di-O-allyl-2-O-benzyl-β-D-mannopyranosid

: 151413-76-2
Octyl-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-(1->6)-2,4-di-O-benzyl-β-D-mannopyranosid

Guidance literature:: Multi-step reaction with 3 steps

2: 77 percent / hydrogenated 1,5-cyclooctadiene-bis(methyldiphenylphosphine)iridium hexafluorophosphate / tetrahydrofuran / 2 h

3: 80 percent / molecular sieves 3 Angstroem, trimethylsilyl triflate / CH₂Cl₂ / 2 h / -20 deg C to r.t.

With trimethylsilyl trifluoromethanesulfonate; 3 A molecular sieve; hydrogenated 1,5-cyclooctadiene-bis(methyldiphenylphosphine)iridium hexafluorophosphate; In tetrahydrofuran; dichloromethane;