2-METHOXY-4-METHYLSULFANYLBENZOYL CHLORIDE

Base Information

Chemical Name:2-METHOXY-4-METHYLSULFANYLBENZOYL CHLORIDE
CAS No.:69883-78-9
Molecular Formula:C₉H₉ClO₂S
Molecular Weight:216.688
Hs Code.:
Mol file:69883-78-9.mol

Synonyms:2-methoxy-4-(methylthio)benzoyl chloride

Suppliers and Price of 2-METHOXY-4-METHYLSULFANYLBENZOYL CHLORIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
2-Methoxy-4-(methylthio)benzoyl chloride 97%
1g
$ 592.00

Atlantic Research Chemicals
2-Methoxy-4-(methylthio)benzoylchloride 95%
1gm:
$ 265.09

Total 3 raw suppliers

Chemical Property of 2-METHOXY-4-METHYLSULFANYLBENZOYL CHLORIDE

Chemical Property:

Melting Point:31°C

Purity/Quality:

99%, ^*data from raw suppliers

2-Methoxy-4-(methylthio)benzoyl chloride 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-METHOXY-4-METHYLSULFANYLBENZOYL CHLORIDE

There total 11 articles about 2-METHOXY-4-METHYLSULFANYLBENZOYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72856-73-6
2-methoxy-4-(methylsulfanyl)benzoic acid

: 69883-78-9
2-methoxy-4-(methylthio)benzoyl chloride

Guidance literature:: With thionyl chloride; In benzene; at 20 - 80 ℃; for 2h;
DOI:10.1016/0223-5234(90)90141-O

Reference yield:

: 4093-29-2
methyl 4-(acetylamino)-o-anisate

: 69883-78-9
2-methoxy-4-(methylthio)benzoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / 10percent NaOH / 3 h / Heating

2: NaNO₂, HCl / H₂O / 0.5 h / 0 - 5 °C

3: 41 percent / Cu / 1.) from 0 deg C to 20 deg C, 3 h, 2.) RT, overnight

4: thionyl chloride / benzene / 2 h / 20 - 80 °C

With hydrogenchloride; sodium hydroxide; thionyl chloride; copper; sodium nitrite; In water; benzene;
DOI:10.1016/0223-5234(90)90141-O

Reference yield:

: 2486-80-8
4-amino-2-methoxybenzoic acid

: 69883-78-9
2-methoxy-4-(methylthio)benzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: NaNO₂, HCl / H₂O / 0.5 h / 0 - 5 °C

2: 41 percent / Cu / 1.) from 0 deg C to 20 deg C, 3 h, 2.) RT, overnight

3: thionyl chloride / benzene / 2 h / 20 - 80 °C

With hydrogenchloride; thionyl chloride; copper; sodium nitrite; In water; benzene;
DOI:10.1016/0223-5234(90)90141-O