methyl 3,5-dibromo-4-(di-tert-butyl((2E,6E,10E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyloxy)silyloxy)benzoate

Base Information

• Chemical Name: methyl 3,5-dibromo-4-(di-tert-butyl((2E,6E,10E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyloxy)silyloxy)benzoate
• CAS No.: 1033756-17-0
• Molecular Formula: C₃₆H₅₆Br₂O₄Si
• Molecular Weight: 740.732

Synonyms:methyl 3,5-dibromo-4-(di-tert-butyl((2E,6E,10E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyloxy)silyloxy)benzoate

Chemical Property of methyl 3,5-dibromo-4-(di-tert-butyl((2E,6E,10E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyloxy)silyloxy)benzoate

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of methyl 3,5-dibromo-4-(di-tert-butyl((2E,6E,10E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyloxy)silyloxy)benzoate

There total 1 articles about methyl 3,5-dibromo-4-(di-tert-butyl((2E,6E,10E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyloxy)silyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Geranylgeraniol (24034-73-9) + methyl 3,5-dibromo-4-hydroxybenzoate (41727-47-3) + di-tert-butylsilyl dibromide (94403-14-2) → methyl 3,5-dibromo-4-(di-tert-butyl((2E,6E,10E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyloxy)silyloxy)benzoate (1033756-17-0)

Guidance literature:

Geranylgeraniol; di-tert-butylsilyl dibromide; With 1H-imidazole; In N,N-dimethyl-formamide; at 20 - 45 ℃; for 4h;

methyl 3,5-dibromo-4-hydroxybenzoate; In N,N-dimethyl-formamide; at 23 ℃; for 5h;

DOI:10.1021/ja801899v

Reference yield: 96.0%

methyl 3,5-dibromo-4-(di-tert-butyl((2E,6E,10E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyloxy)silyloxy)benzoate (1033756-17-0) → 3,5-dibromo-4-(di-tert-butyl((2E,6E,10E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyloxy)silyloxy)benzoic acid (1033756-19-2)

Guidance literature:

With potassium trimethylsilonate; In diethyl ether; at 23 ℃; for 4h;

DOI:10.1021/ja801899v

upstream raw materials:

Geranylgeraniol

methyl 3,5-dibromo-4-hydroxybenzoate

di-tert-butylsilyl dibromide

Downstream raw materials:

3,5-dibromo-4-(di-tert-butyl((2E,6E,10E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyloxy)silyloxy)benzoic acid

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