endo-1,4-epoxy-1,2,3,4-tetrahydro-1-(phenylmethyl)-2,3-anthracenedicarboxylic acid dimethyl ester

Base Information

Chemical Name:endo-1,4-epoxy-1,2,3,4-tetrahydro-1-(phenylmethyl)-2,3-anthracenedicarboxylic acid dimethyl ester
CAS No.:113600-70-7
Molecular Formula:C₂₅H₂₂O₅
Molecular Weight:402.447
Hs Code.:

Synonyms:endo-1,4-epoxy-1,2,3,4-tetrahydro-1-(phenylmethyl)-2,3-anthracenedicarboxylic acid dimethyl ester

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Chemical Property of endo-1,4-epoxy-1,2,3,4-tetrahydro-1-(phenylmethyl)-2,3-anthracenedicarboxylic acid dimethyl ester

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Technology Process of endo-1,4-epoxy-1,2,3,4-tetrahydro-1-(phenylmethyl)-2,3-anthracenedicarboxylic acid dimethyl ester

There total 3 articles about endo-1,4-epoxy-1,2,3,4-tetrahydro-1-(phenylmethyl)-2,3-anthracenedicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 113600-67-2
1,4-epoxy-1,4-dihydro-1-(phenylmethyl)-2,3-anthracenedicarboxylic acid dimethyl ester

: 113600-70-7
endo-1,4-epoxy-1,2,3,4-tetrahydro-1-(phenylmethyl)-2,3-anthracenedicarboxylic acid dimethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 10h; under 2585.7 Torr;
DOI:10.1021/jo00244a001

Reference yield:

: 92878-65-4
1,3-dihydro-1-(phenylmethyl)-1-naphtho<2,3-c>furanol

: 113600-70-7
endo-1,4-epoxy-1,2,3,4-tetrahydro-1-(phenylmethyl)-2,3-anthracenedicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: trichloroacetic acid / toluene / 72 h / Heating

2: 80 percent / H₂ / 5percent Pd/C / ethyl acetate / 10 h / 2585.7 Torr

With hydrogen; trichloroacetic acid; palladium on activated charcoal; In ethyl acetate; toluene;
DOI:10.1021/jo00244a001

Reference yield:

: 762-42-5
dimethyl acetylenedicarboxylate

: 113600-70-7
endo-1,4-epoxy-1,2,3,4-tetrahydro-1-(phenylmethyl)-2,3-anthracenedicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: trichloroacetic acid / toluene / 72 h / Heating

2: 80 percent / H₂ / 5percent Pd/C / ethyl acetate / 10 h / 2585.7 Torr

With hydrogen; trichloroacetic acid; palladium on activated charcoal; In ethyl acetate; toluene;
DOI:10.1021/jo00244a001