3-Phenyl-12,15-dithia-3-phospha-tricyclo[15.4.0.0^5,10]henicosa-1⁽¹⁷⁾,5⁽¹⁰⁾,6,8,18,20-hexaene 3-oxide

Base Information

• Chemical Name: 3-Phenyl-12,15-dithia-3-phospha-tricyclo[15.4.0.0^5,10]henicosa-1⁽¹⁷⁾,5⁽¹⁰⁾,6,8,18,20-hexaene 3-oxide
• CAS No.: 195449-26-4
• Molecular Formula: C₂₄H₂₅OPS₂
• Molecular Weight: 424.568

Synonyms:3-Phenyl-12,15-dithia-3-phospha-tricyclo[15.4.0.0^5,10]henicosa-1⁽¹⁷⁾,5⁽¹⁰⁾,6,8,18,20-hexaene 3-oxide

Chemical Property of 3-Phenyl-12,15-dithia-3-phospha-tricyclo[15.4.0.0^5,10]henicosa-1⁽¹⁷⁾,5⁽¹⁰⁾,6,8,18,20-hexaene 3-oxide

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Technology Process of 3-Phenyl-12,15-dithia-3-phospha-tricyclo[15.4.0.0^5,10]henicosa-1⁽¹⁷⁾,5⁽¹⁰⁾,6,8,18,20-hexaene 3-oxide

There total 6 articles about 3-Phenyl-12,15-dithia-3-phospha-tricyclo[15.4.0.0^5,10]henicosa-1⁽¹⁷⁾,5⁽¹⁰⁾,6,8,18,20-hexaene 3-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Methanesulfonic acid 2-(tert-butyl-dimethyl-silanyloxymethyl)-benzyl ester (151620-08-5) → 3-Phenyl-12,15-dithia-3-phospha-tricyclo[15.4.0.05,10]henicosa-1(17),5(10),6,8,18,20-hexaene 3-oxide (195449-26-4)

Guidance literature:

Multi-step reaction with 5 steps

1: 1.) n-Buli / 1.) THF, 2.) THF

2: aq. H₂O₂

3: HF / acetonitrile

4: SOCl₂ / CH₂Cl₂

5: K₂CO₃ / acetonitrile

With n-butyllithium; thionyl chloride; hydrogen fluoride; dihydrogen peroxide; potassium carbonate; In dichloromethane; acetonitrile;

DOI:10.1021/ja00070a055

Reference yield:

{2-[(2-Hydroxymethyl-benzyl)-phenyl-phosphinoylmethyl]-phenyl}-methanol → 3-Phenyl-12,15-dithia-3-phospha-tricyclo[15.4.0.05,10]henicosa-1(17),5(10),6,8,18,20-hexaene 3-oxide (195449-26-4)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / CH₂Cl₂

2: K₂CO₃ / acetonitrile

With thionyl chloride; potassium carbonate; In dichloromethane; acetonitrile;

DOI:10.1021/ja00070a055

Reference yield:

Bis-[2-(tert-butyl-dimethyl-silanyloxymethyl)-benzyl]-phenyl-phosphane → 3-Phenyl-12,15-dithia-3-phospha-tricyclo[15.4.0.05,10]henicosa-1(17),5(10),6,8,18,20-hexaene 3-oxide (195449-26-4)

Guidance literature:

Multi-step reaction with 4 steps

1: aq. H₂O₂

2: HF / acetonitrile

3: SOCl₂ / CH₂Cl₂

4: K₂CO₃ / acetonitrile

With thionyl chloride; hydrogen fluoride; dihydrogen peroxide; potassium carbonate; In dichloromethane; acetonitrile;

DOI:10.1021/ja00070a055

upstream raw materials:

ethane-1,2-dithiol

C₂₂H₂₁Cl₂OP

Methanesulfonic acid 2-(tert-butyl-dimethyl-silanyloxymethyl)-benzyl ester

phenylphosphane

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