[CoCp₂][Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)]

Base Information

• Chemical Name: [CoCp₂][Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)]
• CAS No.: 1206794-32-2
• Molecular Formula: C₁₀H₁₀Co*C₄₄Br₈F₂₀FeN₅O
• Molecular Weight: 1878.75

Synonyms:[CoCp₂][Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)]

Chemical Property of [CoCp₂][Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)]

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Technology Process of [CoCp₂][Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)]

There total 1 articles about [CoCp₂][Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

cobaltocene (1277-43-6,78206-33-4) + [Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)] (1206794-30-0) → [CoCp2][Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)] (1206794-32-2)

Guidance literature:

In dichloromethane; 1 equiv of Co(C5H5)2 in anhyd. CH2Cl2 was added to a soln. of Fe-complexin CH2Cl2; cold hexane was aded, ppt. was centrifuged, the solid was washed under vac.; elem. anal.;

DOI:10.1021/ja905062w

Reference yield:

[CoCp2][Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)] (1206794-32-2) → [Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)] (1206794-30-0)

Guidance literature:

With CF₃SO₃H; byproducts: H2, CF3SO3(1-), Co(C5H5)2(1+);

DOI:10.1021/ja905062w

upstream raw materials:

cobaltocene

[Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)]

Downstream raw materials:

[Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)]

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