[Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)]

Base Information

• Chemical Name: [Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)]
• CAS No.: 1206794-30-0
• Molecular Formula: C₄₄Br₈F₂₀FeN₅O
• Molecular Weight: 1689.56

Synonyms:[Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)]

Chemical Property of [Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)]

Chemical Property:

Purity/Quality:

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Technology Process of [Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)]

There total 4 articles about [Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato-iron(III) chloride (131917-66-3) → [Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)] (1206794-30-0)

Guidance literature:

2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato-iron(III) chloride; With nitrogen(II) oxide; In methanol; dichloromethane; Inert atmosphere;

for 0.166667h;

DOI:10.1021/ja905062w

Reference yield: 60.0%

2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato-iron(III) chloride (131917-66-3) + nitrogen(II) oxide (10102-43-9) → [Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)] (1206794-30-0)

Guidance literature:

In methanol; dichloromethane; NO was bubbled through a soln. of complex in CH2Cl2 and CH3OH under N2 atm.; the solvent was removed in vac., column chromy. in a drybox (acid alumina, CH2Cl2), the solvent was evapd., the residue was dried under vac.; elem. anal.;

DOI:10.1021/ja905062w

Reference yield:

[CoCp2][Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)] (1206794-32-2) → [Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)] (1206794-30-0)

Guidance literature:

With CF₃SO₃H; byproducts: H2, CF3SO3(1-), Co(C5H5)2(1+);

DOI:10.1021/ja905062w

upstream raw materials:

[CoCp₂][Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)]

2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato-iron(III) chloride

nitrogen(II) oxide

Downstream raw materials:

[CoCp₂][Fe(2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)(NO)]

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