3-Methoxy-5-methylbenzoyl chloride

Base Information

Chemical Name:3-Methoxy-5-methylbenzoyl chloride
CAS No.:96227-40-6
Molecular Formula:C9H9 Cl O2
Molecular Weight:184.61956
Hs Code.:2918990090
DSSTox Substance ID:DTXSID30575973
Wikidata:Q82465470
Mol file:96227-40-6.mol

Synonyms:3-Methoxy-5-methylbenzoyl chloride;96227-40-6;3-METHOXY-5-METHYL-BENZOYL CHLORIDE;SCHEMBL985849;DTXSID30575973

Suppliers and Price of 3-Methoxy-5-methylbenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
3-Methoxy-5-methylbenzoyl chloride 97%
1g
$ 623.00

Atlantic Research Chemicals
3-Methoxy-5-methylbenzoylchloride 95%
1gm:
$ 562.00

Total 4 raw suppliers

Chemical Property of 3-Methoxy-5-methylbenzoyl chloride

Chemical Property:

PSA：26.30000
LogP:2.38260
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:184.0291072
Heavy Atom Count:12
Complexity:170

Purity/Quality:

99%, ^*data from raw suppliers

3-Methoxy-5-methylbenzoyl chloride 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC(=C1)OC)C(=O)Cl

Technology Process of 3-Methoxy-5-methylbenzoyl chloride

There total 5 articles about 3-Methoxy-5-methylbenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62089-34-3
3-methoxy-5-methylbenzoic acid

: 96227-40-6
5-methoxy-3-methylbenzoic acid chloride

Guidance literature:: With thionyl chloride;

Reference yield:

: 585-81-9
3-hydroxy-5-methylbenzoic acid

: 96227-40-6
5-methoxy-3-methylbenzoic acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / 24 h / Heating

2: SOCl₂, DMF / CH₂Cl₂ / 3 h / 23 °C

With sodium hydroxide; thionyl chloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/jo00099a045

Reference yield:

: 33719-74-3
3,5-dichloroanisole

: 96227-40-6
5-methoxy-3-methylbenzoic acid chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Rieke Mg / 1.) THF r.t.; 2.) THF r.t.

2: 1.) Rieke Mg / 1.) THF r.t.; 2.) THF r.t.

3: KOH, H₂O / methanol

4: SOCl₂ / benzene

With potassium hydroxide; thionyl chloride; water; magnesium; In methanol; benzene;
DOI:10.1016/S0040-4039(01)93455-0