(3R,5S)-5-[(1R)-2-(benzyloxy)-1-hydroxyethyl]-3-methyldihydrofuran-2(3H)-one

Base Information

Chemical Name:(3R,5S)-5-[(1R)-2-(benzyloxy)-1-hydroxyethyl]-3-methyldihydrofuran-2(3H)-one
CAS No.:1000050-95-2
Molecular Formula:C₁₄H₁₈O₄
Molecular Weight:250.295
Hs Code.:

Synonyms:(3R,5S)-5-[(1R)-2-(benzyloxy)-1-hydroxyethyl]-3-methyldihydrofuran-2(3H)-one

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Chemical Property of (3R,5S)-5-[(1R)-2-(benzyloxy)-1-hydroxyethyl]-3-methyldihydrofuran-2(3H)-one

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Technology Process of (3R,5S)-5-[(1R)-2-(benzyloxy)-1-hydroxyethyl]-3-methyldihydrofuran-2(3H)-one

There total 11 articles about (3R,5S)-5-[(1R)-2-(benzyloxy)-1-hydroxyethyl]-3-methyldihydrofuran-2(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1067648-41-2
2,3-dideoxy-2-methyl-D-glucono-1,4-lactone

: 100-39-0
benzyl bromide

: 1000050-95-2
(3R,5S)-5-[(1R)-2-(benzyloxy)-1-hydroxyethyl]-3-methyldihydrofuran-2(3H)-one

Guidance literature:: 2,3-dideoxy-2-methyl-D-glucono-1,4-lactone; With di(n-butyl)tin oxide; In toluene; for 5h; Reflux;

benzyl bromide; With tetrabutylammomium bromide; In toluene; at 90 ℃;
DOI:10.1016/j.ejmech.2009.11.013

Reference yield: 79.0%

: 1000050-95-2
(3R,5S)-5-[(1R)-2-(benzyloxy)-1-hydroxyethyl]-3-methyldihydrofuran-2(3H)-one

Guidance literature:

Reference yield: 72.0%

: 127949-92-2
(2R,4E)-6-(benzyloxy)-2-methylhex-4-enoic acid

: 1000050-95-2
(3R,5S)-5-[(1R)-2-(benzyloxy)-1-hydroxyethyl]-3-methyldihydrofuran-2(3H)-one

Guidance literature:: (2R,4E)-6-(benzyloxy)-2-methylhex-4-enoic acid; With tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; In Dimethoxymethane; water; acetonitrile; at 20 ℃; for 0.166667h; Aqueous sodium tetraborate buffer;

With Oxone; edetate disodium; potassium carbonate; In Dimethoxymethane; water; acetonitrile; for 10h;