Technology Process of C24H28Cl4N2P2S
There total 4 articles about C24H28Cl4N2P2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
phosphorus trichloride;
In
tetrahydrofuran;
at -78 - 20 ℃;
for 17h;
Inert atmosphere;
DOI:10.1139/cjc-2013-0015
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ethanol / 20 °C / Inert atmosphere
2: lithium aluminium tetrahydride / diethyl ether / 20 °C / Inert atmosphere
3: phosphorus trichloride / tetrahydrofuran / 17 h / -78 - 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; phosphorus trichloride;
In
tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1139/cjc-2013-0015
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ethanol / 20 °C / Inert atmosphere
2: lithium aluminium tetrahydride / diethyl ether / 20 °C / Inert atmosphere
3: phosphorus trichloride / tetrahydrofuran / 17 h / -78 - 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; phosphorus trichloride;
In
tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1139/cjc-2013-0015