1,4-Methanonaphthalene-2-carboxylicacid,2-amino-1,2,3,4-tetrahydro-,(1alpha,2beta,4alpha)-(9CI)

Base Information

Chemical Name:1,4-Methanonaphthalene-2-carboxylicacid,2-amino-1,2,3,4-tetrahydro-,(1alpha,2beta,4alpha)-(9CI)
CAS No.:91733-74-3
Molecular Formula:C₁₂H₁₃NO₂
Molecular Weight:203.241
Hs Code.:
Mol file:91733-74-3.mol

Synonyms:1,4-Methanonaphthalene-2-carboxylicacid,2-amino-1,2,3,4-tetrahydro-,(1alpha,2beta,4alpha)-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-Methanonaphthalene-2-carboxylicacid,2-amino-1,2,3,4-tetrahydro-,(1alpha,2beta,4alpha)-(9CI)

Chemical Property:

PSA：63.32000
LogP:2.14360

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,4-Methanonaphthalene-2-carboxylicacid,2-amino-1,2,3,4-tetrahydro-,(1alpha,2beta,4alpha)-(9CI)

There total 5 articles about 1,4-Methanonaphthalene-2-carboxylicacid,2-amino-1,2,3,4-tetrahydro-,(1alpha,2beta,4alpha)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 91733-73-2
1,2,3,4-tetrahydro-1,4-methanonaphthalene-2-spiro-5'-hydantoin

: 91733-74-3
2-endo-amino-1,2,3,4-tetrahydro-1,4-methanonaphthalene-2-exo-carboxylic acid

Guidance literature:: With barium dihydroxide; In water; for 70h; Heating;
DOI:10.1039/P19840001283

Reference yield: 79.0%

: 93052-31-4
2-amino-2-carboxamido-1,2,3,4-tetrahydro-1,4-methanonaphthalene

: 91733-74-3
2-endo-amino-1,2,3,4-tetrahydro-1,4-methanonaphthalene-2-exo-carboxylic acid

Guidance literature:: With sulfuric acid; for 5h; Heating;
DOI:10.1039/P19840001283

Reference yield:

: 7374-90-5
3,4-Dihydro-1H-1,4-methano-naphthalen-2-one

: 91733-74-3
2-endo-amino-1,2,3,4-tetrahydro-1,4-methanonaphthalene-2-exo-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / ammonium carbonate / ethanol; H₂O / 5 h / 58 - 60 °C

2: 79 percent / barium hydroxide / H₂O / 70 h / Heating

With ammonium carbonate; barium dihydroxide; In ethanol; water;
DOI:10.1002/jps.2600730408