p-methoxyphenyl 4-O-benzoyl-2,6-dideoxy-6-bromo-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:p-methoxyphenyl 4-O-benzoyl-2,6-dideoxy-6-bromo-2-phthalimido-β-D-glucopyranoside
CAS No.:459170-36-6
Molecular Formula:C₂₈H₂₄BrNO₈
Molecular Weight:582.404
Hs Code.:

Synonyms:p-methoxyphenyl 4-O-benzoyl-2,6-dideoxy-6-bromo-2-phthalimido-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-methoxyphenyl 4-O-benzoyl-2,6-dideoxy-6-bromo-2-phthalimido-β-D-glucopyranoside

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Technology Process of p-methoxyphenyl 4-O-benzoyl-2,6-dideoxy-6-bromo-2-phthalimido-β-D-glucopyranoside

There total 9 articles about p-methoxyphenyl 4-O-benzoyl-2,6-dideoxy-6-bromo-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 138906-43-1
4-methoxyphenyl 4,6-di-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 459170-36-6
p-methoxyphenyl 4-O-benzoyl-2,6-dideoxy-6-bromo-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With N-Bromosuccinimide; barium carbonate; In tetrachloromethane; for 1h; Heating;
DOI:10.1021/ja0127234

Reference yield: 81.0%

: 889453-93-4
p-methoxyphenyl 4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 459170-36-6
p-methoxyphenyl 4-O-benzoyl-2,6-dideoxy-6-bromo-2-phthalimido-β-D-glucopyranoside

Guidance literature:: p-methoxyphenyl 4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside; In 1,1,2,2-tetrachloroethane; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With N-Bromosuccinimide; barium carbonate; In 1,1,2,2-tetrachloroethane; at 100 - 130 ℃; for 3.5h; Molecular sieve; Inert atmosphere;
DOI:10.1055/s-0037-1609719

Reference yield:

: 889453-93-4
p-methoxyphenyl 4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

: C₂₈H₂₃Br₂NO₈

: 459170-36-6
p-methoxyphenyl 4-O-benzoyl-2,6-dideoxy-6-bromo-2-phthalimido-β-D-glucopyranoside

Guidance literature:: p-methoxyphenyl 4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside; In 1,1,2,2-tetrachloroethane; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With N-Bromosuccinimide; barium carbonate; In 1,1,2,2-tetrachloroethane; at 100 - 130 ℃; for 3h; Overall yield = 11.9 g; Molecular sieve; Inert atmosphere;
DOI:10.1055/s-0037-1609719