N-<2-(tert-butoxycarbonyl)hydrazino>carbonyl>phenylalanylleucine

Base Information

Chemical Name:N-<2-(tert-butoxycarbonyl)hydrazino>carbonyl>phenylalanylleucine
CAS No.:102307-08-4
Molecular Formula:C₂₁H₃₂N₄O₆
Molecular Weight:436.508
Hs Code.:

N-<<N<sup>2</sup>-(tert-butoxycarbonyl)hydrazino>carbonyl>phenylalanylleucine

Synonyms:N-<2-(tert-butoxycarbonyl)hydrazino>carbonyl>phenylalanylleucine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-(tert-butoxycarbonyl)hydrazino>carbonyl>phenylalanylleucine

Chemical Property:

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Technology Process of N-<2-(tert-butoxycarbonyl)hydrazino>carbonyl>phenylalanylleucine

There total 3 articles about N-<2-(tert-butoxycarbonyl)hydrazino>carbonyl>phenylalanylleucine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 102307-07-3
N-<2-(tert-butoxycarbonyl)hydrazino>carbonyl>phenylalanylleucine benzyl ester

: 102307-08-4
N-<2-(tert-butoxycarbonyl)hydrazino>carbonyl>phenylalanylleucine

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; for 4h; under 760 Torr;
DOI:10.1021/jm00157a018

Reference yield:

: 870-46-2
t-butoxycarbonylhydrazine

: 102307-08-4
N-<2-(tert-butoxycarbonyl)hydrazino>carbonyl>phenylalanylleucine

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / CHCl₃ / 23 °C

2: 81 percent / N-hydroxybenzotriazole (HOBt) / dimethylformamide / 15 h / 23 °C

3: 92 percent / H₂ / 10percent Pd/C / methanol; dimethylformamide / 4 h / 760 Torr

With hydrogen; benzotriazol-1-ol; triethylamine; palladium on activated charcoal; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm00157a018

Reference yield:

: 102307-06-2
C₁₂H₁₃Cl₃N₂O₄

: 102307-08-4
N-<2-(tert-butoxycarbonyl)hydrazino>carbonyl>phenylalanylleucine

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / N-hydroxybenzotriazole (HOBt) / dimethylformamide / 15 h / 23 °C

2: 92 percent / H₂ / 10percent Pd/C / methanol; dimethylformamide / 4 h / 760 Torr

With hydrogen; benzotriazol-1-ol; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00157a018