2-(4-benzyloxy-2-ethoxycarbonylnaphthalen-1-yl)ethyl triphenylmethyl ether

Base Information

Chemical Name:2-(4-benzyloxy-2-ethoxycarbonylnaphthalen-1-yl)ethyl triphenylmethyl ether
CAS No.:897918-44-4
Molecular Formula:C₄₁H₃₆O₄
Molecular Weight:592.734
Hs Code.:

Synonyms:2-(4-benzyloxy-2-ethoxycarbonylnaphthalen-1-yl)ethyl triphenylmethyl ether

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Chemical Property of 2-(4-benzyloxy-2-ethoxycarbonylnaphthalen-1-yl)ethyl triphenylmethyl ether

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Technology Process of 2-(4-benzyloxy-2-ethoxycarbonylnaphthalen-1-yl)ethyl triphenylmethyl ether

There total 3 articles about 2-(4-benzyloxy-2-ethoxycarbonylnaphthalen-1-yl)ethyl triphenylmethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 897918-40-0
benzyl [4-acetoxy-2-ethoxycarbonylnaphthalen-1-yl]acetate

: 897918-44-4
2-(4-benzyloxy-2-ethoxycarbonylnaphthalen-1-yl)ethyl triphenylmethyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / H₂ / Pd/C / tetrahydrofuran / 2 h / 20 °C / 2844.31 Torr

2: 100 percent / BH₃ / tetrahydrofuran / 1 h / 20 °C

3: 75 percent / pyridine

4: 92 percent / K₂CO₃; ethanol / 4 h / Heating

With ethanol; borane; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; pyridine;
DOI:10.1021/jo060501o

Reference yield:

: 897918-42-2
2-[4-acetoxy-2-ethoxycarbonylnaphthalen-1-yl]ethanol

: 897918-44-4
2-(4-benzyloxy-2-ethoxycarbonylnaphthalen-1-yl)ethyl triphenylmethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / pyridine

2: 92 percent / K₂CO₃; ethanol / 4 h / Heating

With ethanol; potassium carbonate; In pyridine;
DOI:10.1021/jo060501o

Reference yield:

: 897918-41-1
[4-acetoxy-2-ethoxycarbonylnaphthalen-1-yl]acetic acid

: 897918-44-4
2-(4-benzyloxy-2-ethoxycarbonylnaphthalen-1-yl)ethyl triphenylmethyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / BH₃ / tetrahydrofuran / 1 h / 20 °C

2: 75 percent / pyridine

3: 92 percent / K₂CO₃; ethanol / 4 h / Heating

With ethanol; borane; potassium carbonate; In tetrahydrofuran; pyridine;
DOI:10.1021/jo060501o