5'-[2-(2-Benzyloxy-4-methyl-benzoylamino)-ethylcarbamoyl]-[2,2']bipyridinyl-5-carboxylic acid

Base Information

• Chemical Name: 5'-[2-(2-Benzyloxy-4-methyl-benzoylamino)-ethylcarbamoyl]-[2,2']bipyridinyl-5-carboxylic acid
• CAS No.: 204766-02-9
• Molecular Formula: C₂₉H₂₆N₄O₅
• Molecular Weight: 510.549

Synonyms:5'-[2-(2-Benzyloxy-4-methyl-benzoylamino)-ethylcarbamoyl]-[2,2']bipyridinyl-5-carboxylic acid

Chemical Property of 5'-[2-(2-Benzyloxy-4-methyl-benzoylamino)-ethylcarbamoyl]-[2,2']bipyridinyl-5-carboxylic acid

Chemical Property:

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Technology Process of 5'-[2-(2-Benzyloxy-4-methyl-benzoylamino)-ethylcarbamoyl]-[2,2']bipyridinyl-5-carboxylic acid

There total 3 articles about 5'-[2-(2-Benzyloxy-4-methyl-benzoylamino)-ethylcarbamoyl]-[2,2']bipyridinyl-5-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

5'-[2-(2-Hydroxy-4-methyl-benzoylamino)-ethylcarbamoyl]-[2,2']bipyridinyl-5-carboxylic acid ethyl ester (182869-89-2) + 5'-[2-(2-Benzyloxy-4-methyl-benzoylamino)-ethylcarbamoyl]-[2,2']bipyridinyl-5-carboxylic acid ethyl ester (204766-01-8) → 5'-[2-(2-Benzyloxy-4-methyl-benzoylamino)-ethylcarbamoyl]-[2,2']bipyridinyl-5-carboxylic acid (204766-02-9)

Guidance literature:

With sodium hydroxide; In ethanol; Heating;

DOI:10.1002/hlca.19980810203

Reference yield:

benzyl bromide (100-39-0) → 5'-[2-(2-Benzyloxy-4-methyl-benzoylamino)-ethylcarbamoyl]-[2,2']bipyridinyl-5-carboxylic acid (204766-02-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 45 percent / K₂CO₃ / dimethylformamide / Heating

2: 85 percent / NaOH / ethanol / Heating

With sodium hydroxide; potassium carbonate; In ethanol; N,N-dimethyl-formamide;

DOI:10.1002/hlca.19980810203

Reference yield:

5'-[2-(2-Hydroxy-4-methyl-benzoylamino)-ethylcarbamoyl]-[2,2']bipyridinyl-5-carboxylic acid ethyl ester (182869-89-2) → 5'-[2-(2-Benzyloxy-4-methyl-benzoylamino)-ethylcarbamoyl]-[2,2']bipyridinyl-5-carboxylic acid (204766-02-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 45 percent / K₂CO₃ / dimethylformamide / Heating

2: 85 percent / NaOH / ethanol / Heating

With sodium hydroxide; potassium carbonate; In ethanol; N,N-dimethyl-formamide;

DOI:10.1002/hlca.19980810203

upstream raw materials:

5'-[2-(2-Hydroxy-4-methyl-benzoylamino)-ethylcarbamoyl]-[2,2']bipyridinyl-5-carboxylic acid ethyl ester

5'-[2-(2-Benzyloxy-4-methyl-benzoylamino)-ethylcarbamoyl]-[2,2']bipyridinyl-5-carboxylic acid ethyl ester

benzyl bromide

Downstream raw materials:

5'-[2-(2-Benzyloxy-4-methyl-benzoylamino)-ethylcarbamoyl]-[2,2']bipyridinyl-5-carboxylic acid pentafluorophenyl ester

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