2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-glucopyranoside
CAS No.:174149-24-7
Molecular Formula:C₃₂H₃₈O₈Si
Molecular Weight:578.734
Hs Code.:

Synonyms:2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-glucopyranoside

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Chemical Property of 2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-glucopyranoside

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Technology Process of 2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-glucopyranoside

There total 5 articles about 2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 174149-23-6
2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

: 174149-24-7
2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-glucopyranoside

Guidance literature:: With hydrogenchloride; diethyl ether; In tetrahydrofuran; at 0 ℃;
DOI:10.1021/jo951067l

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 174149-24-7
2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / PTSA / acetonitrile / 3 h / 25 °C

2: 96 percent / DMAP / pyridine / 2 h / 25 °C

3: 93 percent / HCl/Et₂O / tetrahydrofuran / 0 °C

With hydrogenchloride; dmap; diethyl ether; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; acetonitrile;
DOI:10.1021/jo951067l

Reference yield:

: 81342-44-1
(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(2-(trimethylsilyl)ethoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 174149-24-7
2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: Amberlite IRA 910 / methanol / 2 h / 25 °C

2: 89 percent / PTSA / acetonitrile / 3 h / 25 °C

3: 96 percent / DMAP / pyridine / 2 h / 25 °C

4: 93 percent / HCl/Et₂O / tetrahydrofuran / 0 °C

With hydrogenchloride; dmap; diethyl ether; Amberlite IRA 910; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; methanol; acetonitrile;
DOI:10.1021/jo951067l