N⁴-(4-methoxy-phenyl)-5-nitro-N²-(1-phenyl-1H-pyrazol-4-yl)-pyrimidine-2,4-diamine

Base Information

• Chemical Name: N⁴-(4-methoxy-phenyl)-5-nitro-N²-(1-phenyl-1H-pyrazol-4-yl)-pyrimidine-2,4-diamine
• CAS No.: 1448694-35-6
• Molecular Formula: C₂₀H₁₇N₇O₃
• Molecular Weight: 403.4

Synonyms:N⁴-(4-methoxy-phenyl)-5-nitro-N²-(1-phenyl-1H-pyrazol-4-yl)-pyrimidine-2,4-diamine

Chemical Property of N⁴-(4-methoxy-phenyl)-5-nitro-N²-(1-phenyl-1H-pyrazol-4-yl)-pyrimidine-2,4-diamine

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Technology Process of N⁴-(4-methoxy-phenyl)-5-nitro-N²-(1-phenyl-1H-pyrazol-4-yl)-pyrimidine-2,4-diamine

There total 2 articles about N⁴-(4-methoxy-phenyl)-5-nitro-N²-(1-phenyl-1H-pyrazol-4-yl)-pyrimidine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-phenyl-1H-pyrazol-4-amine (1128-53-6) + (2-chloro-5-nitro-pyrimidin-4-yl)-(4-methoxy-phenyl)-amine (1331961-87-5) → N4-(4-methoxy-phenyl)-5-nitro-N2-(1-phenyl-1H-pyrazol-4-yl)-pyrimidine-2,4-diamine (1448694-35-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; at 20 ℃; for 16h;

Reference yield:

2-methoxy-phenylamine (90-04-0) → N4-(4-methoxy-phenyl)-5-nitro-N2-(1-phenyl-1H-pyrazol-4-yl)-pyrimidine-2,4-diamine (1448694-35-6)

Guidance literature:

Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 20 °C

2: N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 16 h / 20 °C

With N-ethyl-N,N-diisopropylamine; In 1,4-dioxane;

Reference yield:

N4-(4-methoxy-phenyl)-5-nitro-N2-(1-phenyl-1H-pyrazol-4-yl)-pyrimidine-2,4-diamine (1448694-35-6) → N4-(4-methoxy-phenyl)-N2-(1-phenyl-1H-pyrazol-4-yl)-pyrimidine-2,4,5-triamine (1448694-36-7)

Guidance literature:

With palladium on activated charcoal; hydrogen; In tetrahydrofuran; at 20 ℃; under 760.051 Torr;

upstream raw materials:

2-methoxy-phenylamine

1-phenyl-1H-pyrazol-4-amine

(2-chloro-5-nitro-pyrimidin-4-yl)-(4-methoxy-phenyl)-amine

Downstream raw materials:

N⁴-(4-methoxy-phenyl)-N²-(1-phenyl-1H-pyrazol-4-yl)-pyrimidine-2,4,5-triamine

[3-(4-methoxy-phenyl)-3H-[1,2,3]triazolo[4_,5-d]pyrimidin-5-yl]-(1-phenyl-1H-pyrazol-4-yl)-amine

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