3-(4-phenylpiperazine-1-carbonyl)-N-(4-propylphenyl)benzenesulfonamide

Base Information

Chemical Name:3-(4-phenylpiperazine-1-carbonyl)-N-(4-propylphenyl)benzenesulfonamide
CAS No.:1311383-01-3
Molecular Formula:C₂₆H₂₉N₃O₃S
Molecular Weight:463.601
Hs Code.:

Synonyms:3-(4-phenylpiperazine-1-carbonyl)-N-(4-propylphenyl)benzenesulfonamide

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Chemical Property of 3-(4-phenylpiperazine-1-carbonyl)-N-(4-propylphenyl)benzenesulfonamide

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Technology Process of 3-(4-phenylpiperazine-1-carbonyl)-N-(4-propylphenyl)benzenesulfonamide

There total 4 articles about 3-(4-phenylpiperazine-1-carbonyl)-N-(4-propylphenyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 377769-55-6
C₁₇H₁₉NO₄S

: 4004-95-9,70849-66-0,2210-93-7
1-phenylpiperazine hydrochloride

: 1311383-01-3
3-(4-phenylpiperazine-1-carbonyl)-N-(4-propylphenyl)benzenesulfonamide

Guidance literature:: C₁₇H₁₉NO₄S; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;

1-phenylpiperazine hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 1311383-01-3
3-(4-phenylpiperazine-1-carbonyl)-N-(4-propylphenyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / 12 h / 90 °C / Inert atmosphere

2.1: hydrogenchloride / methanol / 2 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

With hydrogenchloride; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;

Reference yield:

: 77278-63-8
4-phenyl-piperazine-1-carboxylic acid tert-butyl ester

: 1311383-01-3
3-(4-phenylpiperazine-1-carbonyl)-N-(4-propylphenyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / methanol / 2 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide;