C₅₁H₅₅N₄O₁₀P

Base Information

Chemical Name:C₅₁H₅₅N₄O₁₀P
CAS No.:1422958-93-7
Molecular Formula:C₅₁H₅₅N₄O₁₀P
Molecular Weight:914.992
Hs Code.:

C<sub>51</sub>H<sub>55</sub>N<sub>4</sub>O<sub>10</sub>P

Synonyms:C₅₁H₅₅N₄O₁₀P

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₁H₅₅N₄O₁₀P

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Technology Process of C₅₁H₅₅N₄O₁₀P

There total 19 articles about C₅₁H₅₅N₄O₁₀P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1422958-91-5
C₄₂H₃₈N₂O₉

: 124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

: 1422958-93-7
C₅₁H₅₅N₄O₁₀P

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1021/jo302768f

Reference yield:

: 1975-52-6
5-nitro-o-toluic acid

: 1422958-93-7
C₅₁H₅₅N₄O₁₀P

Guidance literature:: Multi-step reaction with 11 steps

1: N-Bromosuccinimide; sulfuric acid / 2.5 h / 60 °C

2: sodium hydroxide; potassium permanganate / water / 60 - 100 °C

3: urea / o-xylene / 4 h / 160 °C

4: tris(pentafluorophenyl)phosphine; triethylamine; palladium diacetate / acetonitrile / 82 °C / Inert atmosphere

5: sodium tris(acetoxy)borohydride / acetonitrile / 1 h / 0 °C / Inert atmosphere

6: pyridine; 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

7: sodium hydrogen sulfide / ethanol; water / 1 h / 78 °C

8: pyridine / 20 °C / Inert atmosphere

9: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 20 °C / Inert atmosphere

10: pyridine / 42 h / 20 °C

11: N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 20 °C

With pyridine; 1H-imidazole; sodium hydrogen sulfide; potassium permanganate; N-Bromosuccinimide; sulfuric acid; palladium diacetate; sodium tris(acetoxy)borohydride; triethylamine tris(hydrogen fluoride); triethylamine; N-ethyl-N,N-diisopropylamine; urea; tris(pentafluorophenyl)phosphine; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; o-xylene; water; N,N-dimethyl-formamide; acetonitrile; 4: |Heck Reaction;
DOI:10.1021/jo302768f

Reference yield:

: 1422958-85-7
3-iodo-5-nitrophthalimide

: 1422958-93-7
C₅₁H₅₅N₄O₁₀P

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydrogen sulfide / ethanol; water / 1 h / 78 °C

2: pyridine; 1H-imidazole / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

3: tris(pentafluorophenyl)phosphine; triethylamine; palladium diacetate / acetonitrile / 82 °C / Inert atmosphere

4: sodium tris(acetoxy)borohydride; acetic acid / acetonitrile / 1 h / 0 °C / Inert atmosphere

5: pyridine / 42 h / 20 °C

6: N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 20 °C

With pyridine; 1H-imidazole; sodium hydrogen sulfide; palladium diacetate; sodium tris(acetoxy)borohydride; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; tris(pentafluorophenyl)phosphine; In tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile; 3: |Heck Reaction;
DOI:10.1021/jo302768f