C₃₂H₃₃N₃O₉

Base Information

Chemical Name:C₃₂H₃₃N₃O₉
CAS No.:1276541-35-5
Molecular Formula:C₃₂H₃₃N₃O₉
Molecular Weight:603.629
Hs Code.:

C<sub>32</sub>H<sub>33</sub>N<sub>3</sub>O<sub>9</sub>

Synonyms:C₃₂H₃₃N₃O₉

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Chemical Property of C₃₂H₃₃N₃O₉

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Technology Process of C₃₂H₃₃N₃O₉

There total 4 articles about C₃₂H₃₃N₃O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1196977-85-1
C₂₅H₂₆N₂O₆

: 1276541-17-3
C₇H₇NO₃

: 1276541-35-5
C₃₂H₃₃N₃O₉

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; at -78 - 0 ℃; for 2h;
DOI:10.1002/ejoc.201001629

Reference yield:

: 1276541-24-2
C₇H₉NO₃

: 1276541-35-5
C₃₂H₃₃N₃O₉

Guidance literature:: Multi-step reaction with 2 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / ethyl acetate / 0.08 h / 20 °C

2: trifluorormethanesulfonic acid / dichloromethane / 2 h / -78 - 0 °C

With trifluorormethanesulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; ethyl acetate;
DOI:10.1002/ejoc.201001629

Reference yield:

: 2450-26-2
2-nitrovanillin

: 1276541-35-5
C₃₂H₃₃N₃O₉

Guidance literature:: Multi-step reaction with 4 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / Reflux

1.2: 0.5 h / 20 °C

1.3: pH 6

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 4 h / 20 °C

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / ethyl acetate / 0.08 h / 20 °C

4.1: trifluorormethanesulfonic acid / dichloromethane / 2 h / -78 - 0 °C

With trifluorormethanesulfonic acid; palladium 10% on activated carbon; hydrogen; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; ethyl acetate;
DOI:10.1002/ejoc.201001629